A Practical Handbook on the Distillation of Alcohol from Farm ProductsWright, F. B. (Frederic B.)
Science
A Practical Handbook on the Distillation of Alcohol from Farm Products
Wright, F. B. (Frederic B.)
Alcohol; Alcohol, Denatured
Another method, which is not to be relied on for very weak liquors, but
which answers well for cordials, wines, and strong ales, is that known as
Brande's method. The liquor is poured into a long, narrow glass tube,
graduated centesimally, until it is half-filled. About 12 or 15 per cent.
of subacetate of lead, or finely powdered litharge, is then added, and
the whole is shaken until all the color is destroyed. Powdered anhydrous
carbonate of potash is next added until it sinks undissolved in the tube,
even after prolonged agitation. The tube is then allowed to rest, when
the alcohol is observed to float upon the surface of the water in a
well-defined layer. The quantity read off on the scale of the tube and
doubled, gives the percentage by volume of alcohol in the original
liquid. The whole operation may be performed in about five minutes, and
furnishes reliable approximative results. In many cases it is necessary
to add the lead salt for the purpose of decolorizing the liquid.
For the investigation of the amount of sugar in, or the concentration of
the mash, or beer, a specially scaled hydrometer is used which is termed
a saccharometer. Sugar possesses a higher degree of specific gravity than
water, and hence it follows that the greater the amount of sugar in the
mash the higher will be the specific gravity. The less the hydrometer
sinks into the fluid the greater the amount of sugar present.
Saccharometers are provided with thermometers whereby the reading may be
corrected to a standard temperature, usually 59∞ F. The saccharometer is
correct for solutions containing sugar alone but it is only approximately
correct for mash liquor which contains a variety of other matters in
variable quantities.
It is a prime necessity that the distiller should be able to determine if
the mash has been completely saccharified by the malt. For this purpose a
solution of iodine is used. Iodine gives to starch a blue color. If the
starch however, has been completely changed into sugar there will either
be no discoloration or the filtered mash liquid which is at first a
yellowish red becomes blue, then violet, and at last red.
=Determination of the Purity of Alcohols.= While the knowledge of the
amount of alcohol contained in a liquid is of great practical utility,
this does not give any idea of the impurities present.
An alcohol of 100 degrees or an absolute alcohol, may contain numerous
impurities which may greatly affect its quality. It is therefore
necessary in addition to analyze the purity of the alcohol.
In commercial practice there are certain simple processes which will give
a basis by which to determine the impurities left after distillation and
rectification. These processes are largely empirical. They are based on
the perception of the senses and are consequently of an entirely relative
degree of precision. Nevertheless, when made by a practical expert, the
operation may give very useful preliminary indications.
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Elsewhere in the archive
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account