A Practical Manual of the Collodion Process, Giving in Detail a Method For Producing Positive and Negative Pictures on Glass and Paper.Humphrey, S. D. (Samuel Dwight)
Science
A Practical Manual of the Collodion Process, Giving in Detail a Method For Producing Positive and Negative Pictures on Glass and Paper.
Humphrey, S. D. (Samuel Dwight)
Ambrotype; Photography
_Remarks._--In the preparation of this sensitive collodion, it is
necessary to be cautious and not add too much of the iodide of potassium
and silver, for in that case the coating would flake off, and falling into
the silvering solution, the operator would be obliged to filter it before
he could silver his plate with safety as regards spotting it.
The method I employ is to add the plain collodion, bromide and iodide of
potassium and silver, iodide of ammonium and hydro-bromic acid, and then
cautiously add the double iodide of potassium and silver from five to
ten drops at a time, trying the collodion from time to time by pouring
a little on a narrow strip of glass, which I dip into the silvering
solution, and let it remain for two minutes. If the coating assumes the
proper color (a cream color), I shake the contents of the bottle, and then
stand it aside to settle: it is better after it has stood for a week or
two.
This collodion I have used after it has been made eight months, and
produced fine and satisfactory results, and use this nearly altogether
in practice. Since the first edition of this work has been issued, I have
sold over two thousand pounds of this preparation, and the demand is on
the increase. I will append another preparation (No. 2) which I have
successfully employed, and some operators prefer.
Bromo-Iodized Collodion for Positives.--No. 2.
Plain collodion 10 ounces.
Iodide of potassium 30 grains.
Bromide of ammonium 20 "
Enough of the double iodide of potassium and silver to give the coating a
cream color when it comes from the silvering solution. It will take from
one to three drachms. Or this last may be omitted, and a few drops of a
saturated solution of dry iodine in alcohol may be added. Either of these
plans have been successful in my practice.
_Remarks._--The iodide of potassium being insoluble in the collodion, it
should be first dissolved in as little water as possible; _i. e._, take
the quantity, 30 grains, put it into a one-ounce graduate, and with a
glass rod stir it, adding water, drop by drop, only until all of the salt
is dissolved. Then it may be poured into the collodion, and there will be
a white powdery precipitate.
The bromide of ammonium will dissolve in the collodion, and can be put
into it. When all of the accelerators are in, it should be well shaken,
and then allowed to settle and become clear. When wanted, a sufficient
quantity may be poured into a vial (see Fig. 34) for use, and the main or
stock bottle should not be disturbed oftener than necessary. This last
collodion is not as durable as the first, but is less trouble to prepare.
Bromo-Iodized Collodion for Negatives.
[Sidenote: IODIZED COLLODION FOR NEGATIVES]
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