A Practical Manual of the Collodion Process, Giving in Detail a Method For Producing Positive and Negative Pictures on Glass and Paper.Humphrey, S. D. (Samuel Dwight)
Science
A Practical Manual of the Collodion Process, Giving in Detail a Method For Producing Positive and Negative Pictures on Glass and Paper.
Humphrey, S. D. (Samuel Dwight)
Ambrotype; Photography
Plain collodion 8 ounces.
Iodide of potassium (dissolved as per page 62) 24 grains.
Bromide of ammonium 16 "
This collodion should be allowed to stand and settle twenty-four hours
before it is used: when wanted, it should be poured off into a collodion
vial. The more free the collodion is from sediment and small particles
of dust or undissolved cotton, the softer and more perfect will be the
impression it makes.
In case the above proportions of iodide of potassium should not produce a
cream-colored coating, when it comes from the nitrate of silver bath, more
may be added: for example, if the coating is of a bluish tint, I would
dissolve 6 grains of iodide of potassium in water, as before, and then try
it: shake well, and test it by putting a little on a slip of glass, and
dipping it into the silvering solution; if it coats to a cream-color, it
is right.
It should be borne in mind, that after the addition of iodide of potassium
here recommended, the collodion should be allowed to stand until settled,
before undertaking to produce a picture, although the coating may be
previously tested by means of a slip of glass.
Solution of Bromide and Iodide of Potassium and Silver.
Dissolve 130 grains of crystallized nitrate, of silver in 4 ounces of
pure water, in a long 8-ounce vial. Then in a clean 1-ounce graduate, or
some other convenient vessel containing half an ounce of water, dissolve
130 grains bromide of potassium. When this and the nitrate of silver are
both dissolved, pour the solution of bromide of potassium into the vial
containing the silver, and a thick yellow precipitate will fall. This
is the bromide of potassium and silver. This should be washed by nearly
filling the vial with water; shake it, and then let it settle, which it
will readily do, and then pour on the water, leaving the yellow mass in
the bottom of the vial; continue this operation of washing for at least
ten changes of water; then, after draining off the water as close as
possible, put into the vial four ounces of alcohol, shake it well and let
it settle; then pour off as close as possible. By this means the water is
nearly all taken out.
Pour into the vial _three_ ounces of alcohol; then in a small mortar
finely pulverize one ounce of iodide of potassium, and the solution, which
was before clear, will be more or less of a yellow color, and the bulk of
the yellow precipitate will be diminished. I have sometimes completely
re-dissolved the yellow precipitate, but this does not often occur, except
there be more water present than is advisable. It is better to have an
excess of bromide of potassium in the solution. This can be seen by its
being white, and remaining undissolved in the bottom of the vial. This
solution should be prepared in the evening, or in a dark room, and only
the light of a lamp or candle employed.
Double Iodide of Potassium and Silver.
Public-domain text, read in full here on John Shaqi.
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