A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purityDeite, C. (Carl)
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A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purity
Deite, C. (Carl)
Cosmetics; Perfumes; Perfumes industry
A filter of simple construction, and performing excellent service, is
shown in Fig. 1. It consists of a large glass bottle, _F_, hermetically
closed by a doubly-perforated cork. The neck of the glass funnel _T_,
the upper rim of which is ground smooth, is placed in one of the holes,
and a glass tube, _r_, bent at a right angle, is fitted into the second
hole. A thick wooden lid, with a rubber ring on the lower side, is
placed upon the funnel, thus closing it air-tight. In the centre of the
lid is fitted a glass tube, _r´_, also bent at a right angle, which is
connected with the tube _r_, by a rubber hose, _k_. After the funnel
has been provided with filtering paper and the oil to be filtered, the
lid is placed upon it, and must not be removed, except for the purpose
of pouring more oil into the funnel. The air in the bottle _F_ is
displaced by the oil dropping into it, and escapes through _r_, _k_ and
_r´_ into the funnel, and thus only the air in the bottle and funnel
can act upon the oil.
The other method for the complete purification of expressed oil is
by rectification or distillation with water. For this purpose the
oil, together with a little water, is brought into one of the stills
described later on, and the oil distilled over. It is sometimes
difficult to obtain the last portion of the oil, especially with a
still heated by direct fire, and it is therefore preferable to combine
it with a fresh quantity of the same oil to be distilled.
_Distillation._--There are at present two methods in use. The one is
founded upon the direct action of the heat, the other upon the use
of steam. The first was formerly in general practice, and is still
largely employed in France and England, and to a limited extent in
this country. It is, however, very deficient in many respects. As the
stills must necessarily be of small capacity, only small quantities
can be distilled at one time, and the oils very rarely possess the
peculiar odor due to them, and sometimes the odor is even altered.
In mixing too little water with the materials to be extracted, there
is danger that empyreumatic oils will be formed; a large quantity of
water, on the other hand, is of disadvantage, in so far as in case
the perfume-materials contain little oil, only a perfumed water, but
no oil, will be obtained. In order to avoid these inconveniences, or,
at least, to do away with some of them, another plan was devised. The
materials to be distilled were spread upon sieves, which were suspended
in the upper part of a still, so that they might be penetrated from
below. It is true no scorching is possible in this case, as was in the
other process when the heating was continued after all the water had
evaporated, and the oil retains its proper color, but by this method
only small quantities can be extracted at a time. The still generally
used for distillation with direct heat resembles so much an ordinary
whiskey still as to need no further description here.
[Illustration: FIG. 2.]
Public-domain text, read in full here on John Shaqi.
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