A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purity — John Shaqi
A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purityDeite, C. (Carl)
History
A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purity
Deite, C. (Carl)
Cosmetics; Perfumes; Perfumes industry
An improved apparatus for distilling dry substances by steam has
been patented in Germany by Messrs. Schimmel & Co., of Leipzic. The
tall conical column at the left (Fig. 6) is the still. About eight
inches from the bottom is a perforated diaphragm or false bottom,
upon which the material to be distilled is placed by introducing it
through the still-head. A perforated coil below the diaphragm projects
steam upwards through the mass, which is occasionally agitated from
without by means of a horizontal stirring apparatus indicated by the
two crosses. Any condensed water which may run back is converted into
steam by the heating coil at the bottom. Meanwhile, the mass itself is
heated by a long coil lining the body of the still and carrying steam
at a high pressure. Whatever of volatile oil is carried forward by the
steam passes through the still-head into the cooler on the right, where
both oil and steam are condensed, and from where they flow through a
small funnel tube into three successive receivers, which are arranged
like Florentine flasks, and which retain the volatile oil that has
separated. From the last receiver the water, which is still impregnated
with oil, enters another reservoir, shown in the illustration only by
dots, and from there it flows into a small globular still situated
underneath; in which, by means of steam, nearly all the oil still
retained is again volatilized with the steam of the water and both
again conducted to the cooler.
[Illustration: FIG. 6.]
Attempts have been made to effect the distillation of volatile
oils without the use of steam by means of hot air, but comparative
experiments have shown that less oil is obtained. With the use of
steam, the vegetable substances swell up by the absorption of water,
and thus afford a free passage to the oil, liberated from the sacs
containing it. With the use of hot air, on the other hand, the surface
of the plant is completely dried and shrivels to a hard solid mass,
which offers considerable resistance to the process of distillation.
This injurious effect of hot air can be somewhat overcome by thoroughly
moistening the plants to be distilled, and allowing the hot air,
before entering the still, to pass through a pipe filled with sponges
constantly kept wet. But this process offers no advantages over that by
steam. The apparatus required is far more complicated; and, besides,
a ventilator has to be provided for forcing the hot air through the
apparatus.
Public-domain text, read in full here on John Shaqi.
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