A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purityDeite, C. (Carl)
History
A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purity
Deite, C. (Carl)
Cosmetics; Perfumes; Perfumes industry
_Separation of the oil and water._--As previously mentioned the
specific gravity of most volatile oils is less than that of water. This
behavior is utilized for the separation of the oil and water, by means
of a so-called Florentine flask (Fig. 7). It consists of a glass flask
provided near the bottom with a pipe, _a_, rising vertically to near
the neck _c_ of the flask where it is bent downwards as shown in the
illustration. The mixed liquid of water and oil drips from the cooling
pipe into the flask, and the water _w_, being specifically heavier,
separates from the oil floating on the top, and gradually ascends in
the pipe _a_, finally flowing over at _d_. Oils specifically heavier
than water are caught in receivers provided with a discharge-pipe near
the mouth of the flask as shown in Fig. 8.
[Illustration: FIG. 7.]
[Illustration: FIG. 8.]
The oil delivered from the receivers is, however, still mixed with
some water, dirt, etc., and for their separation is allowed to stand
quietly for some time. The final separation is effected either by
simply pouring off the oil, especially if larger quantities have to be
handled, or with the assistance of a separator-funnel (Fig. 9). This
consists of the glass-funnel _T_ secured to the stand _G_, and provided
with a close-fitting lid, _P_. The fluid is poured into the funnel, the
lid placed in position, and the whole allowed to rest until the water
_W_ is completely separated from the oil _O_. The oil is then separated
from the last drops of water by carefully opening the faucet _H_.
Most volatile oils are obtained by distillation, but this method is
not practicable for separating the odoriferous principle of many of the
most sweet-scented and delicate flowers, partially because the flowers
contain too little oil, and partially because the oil would lose in
quality if obtained by distillation.
[Illustration: FIG. 9.]
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