A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purityDeite, C. (Carl)
History
A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purity
Deite, C. (Carl)
Cosmetics; Perfumes; Perfumes industry
_Extraction._--For obtaining the volatile oils by extraction various
solvents such as ether, bisulphide of carbon, etc., may be employed.
Carefully rectified petroleum-ether is very suitable for the purpose.
It completely evaporates at about 122° F., and when sufficiently
purified does not possess a disagreeable odor. The process of
extraction is briefly as follows: The material to be extracted is
treated in a digester with petroleum-ether or one of the above-named
solvents. The solution is then drawn off and the solvent evaporated
in a still. The recondensed solvent flows immediately back into the
digester and further extracts the material contained therein. The
operation is repeated until nothing soluble remains. In practice some
difficulties are, however, connected with this process since, besides
the volatile oils, resins, and coloring and extractive substances are
dissolved, which have to be removed, as well as the last traces of the
solvent, as otherwise the oil would acquire a foreign odor. Further
the solvents mentioned are very volatile and inflammable, requiring
the greatest precautions as regards fire. For these reasons the
extraction process is not suitable for many purposes, and though at
first great hopes were entertained in regard to it, its use is limited
to substances with a large content of volatile oil.
[Illustration: FIG. 10.]
For extraction on a small scale, the apparatus, Fig. 10, is a very
suitable one. It is especially adapted for manufacturers of perfumery,
who wish to extract fresh flowers. It consists of a cylindrical vessel,
_C_, of tin plate, provided on the bottom with the stop-cock _a_ and
the pipe _b_. The lid _D_ fits into a gutter, _R_, running around the
edge of _C_, and is hermetically closed by water in _R_. The cylinder
is filled with the vegetable substance to be extracted, and sufficient
petroleum-ether or bisulphide of carbon to cover it, poured in. The lid
is then adjusted, the gutter _R_ filled with water and the apparatus
allowed to stand quietly for forty minutes. To remove the fluid from
the cylinder, the faucet _o_ in the lid is first opened, and then the
stop-cock _a_; the fluid escapes at _b_, and is caught in a well-closed
vessel. The operation may be repeated once or twice, or the vegetable
substance is pressed out by means of a wooden plate, and the apparatus
filled anew. The faucet _h_ serves for emptying the gutter _R_.
[Illustration: FIG. 11.]
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