A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purity — John Shaqi
A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purityDeite, C. (Carl)
History
A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purity
Deite, C. (Carl)
Cosmetics; Perfumes; Perfumes industry
For the extraction of oil on a larger scale, the apparatus shown in
Fig. 13 is very suitable. It consists of two principal parts, the
actual extracting vessel _E_, and the still _B_. The extracting vessel
_E_ sits in a vat containing cold water, _W_, the arrangement being
such that the heated water can be removed and replaced by cold. The
still _B_ sits in a boiler, _K_, filled with hot water.
The apparatus is charged as follows: The conical head _C_ of the
extracting vessel _E_ is unscrewed and its connection at _H_ with the
pipe _R_ loosened. The extracting vessel is then charged with the
vegetable substance, the head _C_ replaced, and the connection with the
pipe _R_ restored. The cocks _H_{2} and _H_{4} are then opened, and
the required quantity of solvent is brought into the still. Both cocks
are then closed, and the cocks _H_ and _H_{1} opened. The water in the
boiler is then heated until the contents of the still commence to boil.
The vapor of the solvent ascends through the pipe _R_; on entering the
extracting vessel _E_ it is condensed, and after falling as a spray
upon the material to be extracted, finally returns impregnated with
volatile oil to the still _B_. Here the solvent is revaporized, and
passes again through the material in the extracting vessel, while the
extracted oil remains in the still. During the boiling of the solvent
the extracting vessel must be suitably cooled by the constant admission
of cold water.
[Illustration: FIG. 13.]
When extraction is finished, the cocks _H_ and _H_{1} are closed, and
the cock _H_{2}, which is connected with a cooling worm, is opened.
The solvent is then evaporated, and regained by condensation. The oil
is discharged, from the still through a pipe in the bottom provided
with the cock _H_{3}.
The apparatus may also be so arranged that the still _B_ is connected
with two extracting vessels which are used alternately, while the
contents of one are being extracted the other is emptied and refilled.
[Illustration: FIG. 14.]
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