A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purityDeite, C. (Carl)
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A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purity
Deite, C. (Carl)
Cosmetics; Perfumes; Perfumes industry
For working on a very large scale, Heyl's extracting apparatus, shown
in Fig. 14, is very suitable. It consists of a battery of four or more
cast iron or sheet iron cylinders, _A_{1} to _A_{4}, communicating
with each other and surrounded by steam jackets. The extracting
vessels are so arranged that they can be emptied by tilting, which is
rather inconvenient, as all the pipes have to be unscrewed. In each
cylinder close above the bottom is a perforated plate covered with
fine wire-gauze, upon which the material to be extracted is placed.
The cylinder is filled to the top, and, after placing a similar plate
upon it, the upper opening is closed by a lid suspended to a crane. The
cylinder, as well as the lid, is provided with a broad flange, between
which is placed a hemp tissue firmly pressed together by 12 clamps to
serve for packing. After filling the cylinders with the material to be
extracted and arranging the packing, the solvent (bisulphide of carbon)
is conducted from a reservoir through the principal pipe, _B_, to the
extracting vessels, and is introduced into _A_{2} by opening the cock
_C_{2}, which communicates with the pipe _B_. The bisulphide of carbon
passes through the bent pipe _D_{1}, enters through the cock _E_{2},
below the false bottom of the cylinder _A_{2}, and, after penetrating
the mass and filling the cylinder, runs through the cock _C_{2} of
the bent pipe _D_{2}, and the cock _E_{3} into the cylinder _A_{3},
reaching the fourth cylinder in the same manner through the cock
_C_{3}, the pipe _D_{3}, and the cock _E_{4}. From the last cylinder
it passes as a thoroughly saturated oil solution into a reservoir, in
which a vacuum has been created to promote the circulation of the fluid
in the entire apparatus. After a quantity of oil solution corresponding
to the contents of the cylinder _A_{4} has arrived, the cock _G_{4}
is closed and the cock _C_{4} opened, whereby the cylinder _A_{4} is
connected with _A_{1} by the bent pipe _D_{4} and the cock _E_{1}.
After the exhaustion of the contents of the cylinder _A_{2}, which
is recognized by means of the glass tube _H_{2} placed on _D_{2} by
the fluid running off being colorless, the cocks _C_{1} and _E_{2}
are closed, and _C_{2} and _E_{3} opened, whereby the solvent runs
into _A_{3}, and from there to _A_{4} and _A_{1}; _A_{2} being
omitted. To effect this omission, and at the same time not to prevent
the introduction of bisulphide of carbon, _C_{1}, _C_{2}, _C_{3},
and _C_{4}, are so-called two-way cocks, which, when placed in one
position, connect the principal pipe _B_ with the branch pipes _D_, but
interrupt a further flow through the principal pipe _B_; while in the
other position they close the pipes _D_ and open the principal pipe _B_.
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