A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purityDeite, C. (Carl)
History
A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purity
Deite, C. (Carl)
Cosmetics; Perfumes; Perfumes industry
The cylinder _A_{2} is, however, still filled with the solvent and
material saturated with it. To remove the solvent, the discharge cock
_K_{2} on the bottom of the cylinder is opened, which communicates
with the discharge pipe _J_, through which the bisulphide of carbon
is conducted into a reservoir. The discharge is promoted by opening
the cock _M_{2}, connected with the pipe _L_, and the admittance of
compressed air, which displaces the liquid solvent. After the flow
of the latter has ceased, the steam cocks on the jacket _O_{2} and
the cylinder _P_{2} are opened under constant admission of air and
simultaneous introduction of steam through the pipe _N_ into the upper
part of the cylinder.
The solvent (bisulphide of carbon) converted into vapor by the heat,
is conducted together with the aqueous vapor, by the admission of air
through the cock _K_{2}, the pipe _J_, and a cooling pipe placed
between the extracting vessels and the reservoir, and collected in a
reservoir to be re-used.
On account of the great volatility of bisulphide of carbon,
considerable loss would, however, be incurred by the above-mentioned
admission of air. To avoid this, the reservoir serving for the
reception of the condensed bisulphide of carbon and aqueous vapor
is closed, and connected by a pipe with a long, narrow, horizontal
cylinder half filled with oil, and provided with a fan-shaft. The
vapors of bisulphide of carbon entering the cylinder from the reservoir
are absorbed, together with the air by the oil, the surface of which is
constantly agitated by the fan-shaft, while the air, rendered entirely
inodorous, passes out at the other end. The bisulphide of carbon is
finally separated from the oil by distillation and again used.
After the cylinder _A_{2} is sufficiently steamed, it is emptied and
again charged with material and connected with the cylinder _A_{1};
while the other cylinders undergo the same manipulations described
above.
[Illustration: FIG. 15.]
The saturated oil solution is subjected to distillation, which is
readily effected in Heyl's apparatus, Fig. 15. The lower part of the
still _A_ of boiler plate is surrounded by the steam-jacket _B_, into
which steam is admitted through _C_ and the condensed water discharged
through _D_. The concentrated oil solution runs from a reservoir,
standing at a higher level through the pipe _E_ into the still, the
admission of a sufficient quantity being indicated by the gauge _F_.
The bisulphide of carbon brought to the boiling point (114° F.) by the
steam introduced into the jacket, vaporizes quickly; the vaporization
being still more accelerated by revolving the stirrer _H_, by means of
the crank _G_. The vapors of bisulphide of carbon escape through four
openings in the upper part of the still, into a capacious worm, the
lower part of which enters, under water, a reservoir.
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