A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purityDeite, C. (Carl)
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A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purity
Deite, C. (Carl)
Cosmetics; Perfumes; Perfumes industry
An adulteration with _fat oil_ (poppy oil, castor oil) may be
recognized as follows: Place a drop of the suspected oil upon blotting
paper and expose it to the heat of the water bath. If it evaporates
completely and no stain is perceptible, the oil is pure. But frequently
a transparent stain remains with old oils without their being
adulterated, which is due to the resin formed by the absorption of
oxygen and remaining dissolved in the oil. In this case a transparent
ring is generally formed by the concentration of the resin on the
edges of the stain. If no tangible results are obtained by this test,
pour a few cubic centimeters of the oil upon a watch-crystal and
heat it very slowly upon a piece of sheet-iron, until all the odor
has disappeared. If the watch-crystal becomes empty in a short time,
nothing but volatile oil was present; but if a viscous residue remains,
this may consist either of fatty oil or resin, or of both. Treat the
residue with strong alcohol; if it dissolves it may be resin or castor
oil. Dilute the solution with much water; a white flocculent turbidity
indicates resin; the separation of an oily liquid, after standing,
castor oil. If the residue remains undissolved, it consists of a fatty
oil, generally oil of almond or olive.
The presence of castor oil can be accurately determined by bringing
the residue from the watch-crystal into a test-tube by means of a
glass-rod, and compounding it with a few drops of nitric acid. A
strong development of gas takes place, after the cessation of which,
solution of carbonate of soda is added as long as there is any sign
of effervescence. If the added oil was castor oil, the contents of the
test-tube will show a peculiar odor due to œnanthylic acid formed by
the action of nitric acid upon castor oil.
Another method of establishing the presence of fat oil consists in
mixing the suspected oil with eight times its quantity of 90 per
cent. alcohol (specific gravity 0.823). If the oil is unadulterated a
clear solution is formed; if it contains fat oil, the latter remains
undissolved. The presence of castor oil, which of the fat oils is
chiefly used for adulteration, is, however, not shown by this method,
it being also soluble in alcohol.
A permanent stain upon the paper may, however, also be formed by fresh
oils obtained by expression from the respective parts of the plant.
Thus, lemon oil obtained by expression from the peel, and which has
a far more agreeable odor than that produced by distillation, always
leaves behind a slight grease-stain.
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