A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purity — John Shaqi
A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purityDeite, C. (Carl)
History
A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purity
Deite, C. (Carl)
Cosmetics; Perfumes; Perfumes industry
_Detection of alcohol or spirit of wine._--Independent of the alcohol
added to assist the preservation of some oils, adulteration with
alcohol frequently occurs, especially in expensive oils. With a content
of not more than 3 per cent. of alcohol, it suffices to allow one to
two drops of the suspected oil to fall into water. In the presence of
alcohol, the drop becomes either immediately surrounded with a milky
zone, or it becomes turbid or whitish after being for some time in
contact with the water. Dragendorff's test is based upon the fact
that oils, which are hydrocarbons, suffer no change by the addition
of sodium (ten drops of oil and a small chip of sodium), while oils
containing hydrocarbons and oxygenated oils cause with sodium a slight
evolution of hydrogen gas, and suffer but a slight change during the
first five to ten minutes of the reaction. If, however, the oil is
adulterated with alcohol, not only a violent evolution of hydrogen gas
takes place, but the oil in a short time becomes brown or dark brown,
thickly fluid or rigid.
The detection of alcohol by means of fuchsine, which has been
frequently recommended, requires special precautions. It must first
be ascertained that the oil is free from acids and water; if such
is not the case, they must be removed by means of caustic potash.
After settling, bring, by means of a dry pipette, about five cubic
centimeters of the oil into a dry test-tube about ten millimeters
in diameter, without moistening the walls of the upper half of the
tube. Then bring, by means of a paper gutter, a few milligrammes of
coarsely-powdered fuchsine into the dry part of the obliquely held
tube, at a distance of one centimeter from the oil. Now heat gradually
over a lamp until the tube begins to tarnish. With pure oil no
evaporation is observed, but if the oil contains only 0.1 per cent.
of alcohol, every speck of fuchsine will, after heating to boiling
and setting aside, be surrounded by a stain produced by the alcoholic
solution. The chief requirement for this test is that the oil be free
from water. If such is not the case, vapors will be observed, which
condense in the upper portion of the test-tube, and dissolve fuchsine,
and, after flowing back, sink below the oil with a crackling noise. If
the oil contains alcohol, the condensing vapors dissolve fuchsine with
greater ease, and in flowing back mix without crackling.
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