A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purityDeite, C. (Carl)
History
A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purity
Deite, C. (Carl)
Cosmetics; Perfumes; Perfumes industry
Wintergreen oil is also obtained by distillation from _Gaultheria
punctata_ and _Gaultheria leucocarpa_. An oil, very closely resembling
wintergreen oil, is in this country distilled from the young shoots of
the American species of birch, _Betula lenta_, variously called sweet
birch, black birch, cherry birch, and mountain mahogany. According
to Procter, the oil does not exist in the birch but is formed by the
action of the water upon an odorless body, called gaultherin, which
is converted into volatile oil by the reaction of another substance
analogous to emulsin. Hence the formation of oil is similar to that
of oil of bitter almonds. To obtain the oil from _Betula lenta_,
the material is chopped up and placed in the still, as much as this
will hold, a sufficient quantity of water being then added to fill
the still about one-third full. The still is generally permitted to
remain in this condition over night, a fire is made in the morning
and distillation proceeds nicely. The manufacture of birch oil is
carried on at quite a large scale by Mr. A. H. Seidle, of Middleport,
Schuylkill County, Pa.
Methyl salicylate may also be artificially prepared by heating a
mixture of methyl alcohol, sulphuric acid and salicylic acid whereby
at first methyl-sulphuric acid is formed which is then converted into
methyl ether and sulphuric acid:--
{OH {OCH_{3}
SO_{2}{ + CH_{3}OH = SO_{2}{ + H_{2}O
{OH {OH
{OCH_{3} {OH
SO_{2}{ + C_{6}H_{4}{ =
{OH {COOH
{OH {OH
C_{6}H_{4}{ + SO_{2}{
{CO.OCH_{3} {OH.
Etherification succeeds without difficulty, it being sufficient to
heat the mixture for some time and then pour it into water whereby
the ether separates as a heavy layer of oil. After washing with water
distil in a direct current of steam. The ether thus obtained is as
clear as water and, as regards its other properties, does not differ
from the naturally occurring oil. This artificial wintergreen oil is
now much used for perfuming purposes.
Wintergreen oil is said to be frequently adulterated with sassafras oil
which is also specifically heavier than water. If, according to Hayer,
5 drops of the oil in a test-tube be mixed with 10 drops of crude
concentrated nitric acid, a deep blood-red fluid results in one minute
if oil of sassafras is present. In the course of another minute, the
fluid separates a brown resinous mass. Pure oil, on the other hand, is
but little altered.
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Elsewhere in the archive
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account