A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic CombinationsAnonymous
Science
A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations
Anonymous
Blowpipe
Mineral. Glance cobalt
Formula. CoS^{2} + CoAs.
Behavior
(1) in glass-bulb. --
(2) in open tube. As the preceding, but gives off more SO^{2}.
(3) on charcoal. Gives off S and As, and fuses to a magnetic
bead. Colors flame blue.
(4) in forceps. --
(5) in borax. Gives a cobalt and slight iron reaction when
treated as the preceding minerals.
(6) in mic. salt. As in borax.
(7) with carb. soda. Gives a sulphur reaction of silver.
(8) Special reactions. As the preceding.
* * * * *
Mineral. Nickel glance
Formula. NiS^{2} + NiAs.
Behavior
(1) in glass-bulb. Decrepitates and gives an orange colored
sublimate of AsS^{2}.
(2) in open tube. As the preceding.
(3) on charcoal. As the preceding.
(4) in forceps. --
(5) in borax. As copper nickel.
(6) in mic. salt. Gives the nickel reaction occasionally somewhat
obscured by cobalt.
(7) with carb. soda. As the preceding.
(8) Special reactions. As copper nickel.
* * * * *
Mineral. Ulmannite
Formula. NiS^{2} + Ni(AsSb)^{2}.
Behavior
(1) in glass-bulb. Gives a slight white sublimate of SbO^{3} and
more or less AsS^{3}.
(2) in open tube. Gives off thick fumes of SbO^{3} and SbO^{5}
with AsO^{3} and SO^{2}.
(3) on charcoal. As glance cobalt, but accompanied by dense fumes
of SbO^{3}.
(4) in forceps. --
(5) in borax. As copper nickel.
(6) in mic. salt. As the preceding.
(7) with carb. soda. As the preceding.
(8) Special reactions. As copper nickel generally, but arsenic is not
always present.
* * * * *
Mineral. Cobalt pyrites
Formula. ([,Co][,Ni][,Fe]) ([,,,Co=][,,,Ni=][,,,Fe=]).
Behavior
(1) in glass-bulb. When strongly heated gives off sulphur and
becomes brown.
(2) in open tube. Gives off much SO^{2} and a small quantity of
AsO^{3}.
(3) on charcoal. In the reducing flame small fragments fuse with
the evolution of sulphur to a magnetic bead
having a bronze colored fracture.
(4) in forceps. --
(5) in borax. In the oxidizing flame on charcoal gives a
violet colored glass. In the reducing flame the
nickel is reduced and may collected in a gold
bead. When the nickel is removed, the glass
exhibits a slight iron reaction while warm.
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