A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic CombinationsAnonymous
Science
A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations
Anonymous
Blowpipe
In places where the proper kind of charcoal is difficult to procure,
it is economical to cut common charcoal into pieces about an inch
broad, and the third of an inch thick. In each of these little pieces
small cavities should be cut with the small end of the borer. When
these pieces of charcoal are required for use, they must be fastened
to a narrow slip of tin plate, one end of which is bent into the form
of a hook, under which the plate of charcoal is pushed.
In general, we use the charcoal support where we wish to reduce
metallic oxides, to prevent oxidation, or to test the fusibility of a
substance. There is another point to which we would direct the
student. Those metals which are volatile in the reduction flame,
appear as oxides in the oxidation flame. These oxides make sublimates
upon the charcoal close in the vicinity of the substance, or where it
rested, and by their peculiar color indicate pretty correctly the
species of minerals experimented upon.
(_b._) _Platinum Supports._--The metal platinum is infusible in the
blowpipe flame, and is such a poor conductor of heat that a strip of
it may be held close to that portion of it which is red hot without
the least inconvenience to the fingers. It is necessary that the
student should be cognizant of those substances which would not be
appropriate to experiment upon if placed on platinum. Metals should
not be treated upon platinum apparatus, nor should the easily
reducible oxides, sulphides, nor chlorides, as these substances will
combine with the platinum, and thus render it unfit for further use in
analysis.
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