A text-book of assaying : $b for the use of those connected with mines.Beringer, C. (Cornelius)
Science
A text-book of assaying : $b for the use of those connected with mines.
Beringer, C. (Cornelius)
Assaying
The method of determining sp. g. with the hydrometer is obviously
inapplicable to the case of solids, and in the case of liquids it should
not be used where exact figures are required. There are several other
methods which may be used, but on the whole those with the specific
gravity bottle are most convenient.
[Illustration: FIG. 35.]
~The specific gravity bottle~ (fig. 35) is a light flask of about 25
c.c. capacity, provided with a well-fitting perforated stopper. It is
essentially a graduated flask, which measures a constant volume, but it
does not much matter what the volume is.
_In taking the sp. g. of a liquid_ (_or, what is the same thing, a fused
solid_) there is wanted the weights (1) of the flaskful of water and (2)
of the flaskful of the liquid. Dividing the second by the first gives
the required sp. g. The actual weighings required are--
(1) of the dry and empty flask,
(2) of the flask filled with water, and
(3) of the flask filled with the liquid.
The weighing of the flask once made need not be often repeated. It is
well to do so now and then for safety's sake; but one weighing will
serve for a large number of determinations. The same remarks apply to
the weighing of the bottle filled with water. The bottle is dried by
rinsing out first with alcohol and afterwards with ether; ether is very
volatile, and a short exposure in a warm place will soon drive off the
little remaining about the sides. The ether vapour should be sucked out
through a glass tube. See that the bore of the stopper is dry as well as
the bottle. Let the dry bottle stand in the box of the balance for a
minute or two before weighing. The weight is, strictly speaking, not
that of the empty bottle, but of the bottle filled with air. The empty
bottle would weigh from 20 to 30 milligrams less. Correcting for this
would, in most cases, only make a difference in the fourth place of
decimals,[8] so that it is better to ignore the error.
The weight of the flask filled with water is got by filling it with
distilled water, and inserting the stopper. The excess of water will
overflow at the margin and through the bore. The bottle is wiped with a
soft, dry cloth, taking care not to squeeze or warm the bottle. The
bottle will remain filled to the top of the stopper. It is allowed to
stand in the balance box for a minute or two, and then weighed.
Distilled water, as stated, should be used; the use of ordinary water
may increase the weight by 5 or 6 milligrams. Many waters, if they have
not previously been boiled, give off bubbles of air which render the
weighing worthless.
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Elsewhere in the archive
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account