Cooley's Cyclopædia of Practical Receipts and Collateral Information in the Arts, Manufactures, Professions, and Trades..., Sixth Edition, Volume ICooley, Arnold James
Science
Cooley's Cyclopædia of Practical Receipts and Collateral Information in the Arts, Manufactures, Professions, and Trades..., Sixth Edition, Volume I
Cooley, Arnold James
Formulas, recipes, etc.; Industrial arts -- Dictionaries; Technology -- Dictionaries
The preparation of pure solution of ammonia admits of no other
improvements than such as merely affect the form of the apparatus employed
to produce it; and hence, unlike the ammonia-salts of commerce, has been
little meddled with by inventors and patentees. Among the plans having for
their object the production of an ammoniacal solution, more or less
concentrated, fitted for many of the purposes of the arts, and for the
preparation of salts, but not for chemical and medical use, besides those
of Reece, Spence, Crane and Jullien, &c., already noticed, may be
mentioned——
1. That of Watson (Patent dated 1838) in which gas-liquor mixed with a
proper quantity of fresh-slaked lime is distilled from a spacious retort
or still into a receiver containing cold water, until much steam passes
over with the gas, when the strong alkaline liquor forming the distillate,
and called the first portion, is drawn off. The distillation is then
continued, when a weaker and impurer solution is obtained, called the
second portion. The first portion is then reintroduced into a retort or
still with a small quantity of fresh lime, and the distillation repeated.
The product the patentee calls the first portion of the second
distillation. The latter is a strong ammoniacal liquor sufficient for all
the purposes of scouring, cleaning, conversion into commercial
ammonia-salts, &c. It may be further purified by a third distillation; the
second portion of each operation being transferred again to the still with
the next fresh charge of gas-liquor.
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