Detection of the Common Food AdulterantsBruce, Edwin M.
Science
Detection of the Common Food Adulterants
Bruce, Edwin M.
Food adulteration and inspection
FATS AND OILS 60
=Lard=--Adulterations of--Cottonseed oil--Cottonseed stearin--Beef
stearin.
=Olive Oil=--Adulterations of--General test--Cottonseed oil--Peanut
oil--Sesame oil--Rape oil.
CHAPTER XII
BEVERAGES 65
=Coffee=--Adulterations of--General test--Coloring matter--
Imitation coffee beans--Chicory.
=Tea=--Adulterations of--Foreign leaves--Exhausted tea leaves--Lie
tea--Facing--Catechu.
PURE FOOD TESTS
CHAPTER I
DAIRY PRODUCTS
MILK
Milk is adulterated by watering, removing the cream or by adding some
foreign substance. Formaldehyde, boric acid or salicylic acid may be
added to preserve the milk. Annatto, caramel or some coal-tar dye is
added, sometimes to improve the color of the milk, and at other times to
cover up traces of watering. Gelatin and starch are added for the same
purpose, though they are not frequently used.
ARTIFICIAL COLORING MATTER
ANNATTO
Add acid sodium carbonate to a sample of the milk until it shows a
slight alkaline reaction. Immerse a piece of filter-paper and leave it
in for 12 or 15 hours. If annatto is present, there will be a
reddish-yellow stain on the paper.
CARAMEL
_Leach’s Method._--Warm 150 cc. of the sample and add 5 cc. of acetic
acid, then continue heating it nearly to the boiling point, stirring
while it is being heated. Separate the curd by gathering it with the
stirring rod or by pouring through a sieve. Press out all the whey from
the curd and macerate the latter for several hours (10 to 12 hours) in
50 cc. of ether. It is best to do this in a tightly corked flask,
shaking it frequently. If the milk was uncolored or colored with annatto
the curd when thus treated will be white. If the curd is a dull brown
color caramel was probably used to color the milk. Confirm its presence
by shaking a portion of the curd with concentrated hydrochloric acid
(sp. gr. 1.20) and gently heating. If the acid solution turns blue while
the curd does not change its color, caramel was used to color the milk.
(Remember that the ether-extracted curd must be brown.)
COAL TAR COLORS
_Lythgoe’s Method._--Mix in a porcelain vessel about 15 cc. each of the
sample of milk and hydrochloric acid (sp. gr. 1.20) and break up the
curd into coarse lumps by shaking gently. If an azo-color was used to
color the milk this curd will be pink, but the curd of normal milk will
be white or yellowish.
STARCH
The presence of starch in milk may be detected by heating a small
quantity of the milk to boiling. When it has cooled add a drop of iodin
in potassium iodid, and if starch is present there will be a blue
coloration.
GELATIN
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