Elements of Chemistry,: In a New Systematic Order, Containing all the Modern DiscoveriesLavoisier, Antoine Laurent
Science
Elements of Chemistry,: In a New Systematic Order, Containing all the Modern Discoveries
Lavoisier, Antoine Laurent
Chemistry -- Early works to 1800
All these precautions are solely intended for collecting and determining
the quantity of water formed during the experiment; the carbonic acid
and azotic gas remains to be ascertained. The former is absorbed by
caustic alkaline solution in the bottles 22 and 25. I have only
represented two of these in the figure, but nine at least are requisite;
and the last of the series may be half filled with lime-water, which is
the most certain reagent for indicating the presence of carbonic acid;
if the lime-water is not rendered turbid, we may be certain that no
sensible quantity of that acid remains in the air.
The rest of the air which has served for combustion, and which chiefly
consists of azotic gas, though still mixed with a considerable portion
of oxygen gas, which has escaped unchanged from the combustion, is
carried through a third tube 28, 29, of deliquescent salts, to deprive
it of any moisture it may have acquired in the bottles of alkaline
solution and lime-water, and from thence by the tube 29, 30, into a
gazometer, where its quantity is ascertained. Small essays are then
taken from it, which are exposed to a solution of sulphuret of potash,
to ascertain the proportions of oxygen and azotic gas it contains.
In the combustion of oils the wick becomes charred at last, and
obstructs the rise of the oil; besides, if we raise the wick above a
certain height, more oil rises through its capillary tubes than the
stream of air is capable of consuming, and smoke is produced. Hence it
is necessary to be able to lengthen or shorten the wick without opening
the apparatus; this is accomplished by means of the rod 31, 32, 33, 34,
which passes through a leather-box, and is connected with the support of
the wick; and that the motion of this rod, and consequently of the wick,
may be regulated with the utmost smoothness and facility; it is moved at
pleasure by a pinnion which plays in a toothed rack. The rod, with its
appendages, are represented Pl. XII. Fig. 3. It appeared to me, that the
combustion would be assisted by surrounding the flame of the lamp with a
small glass jar open at both ends, as represented in its place in Pl.
XI.
Public-domain text, read in full here on John Shaqi.
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