Elements of the Theory and Practice of Chymistry, 5th ed.Macquer, Pierre Joseph
History
Elements of the Theory and Practice of Chymistry, 5th ed.
Macquer, Pierre Joseph
Chemistry -- Early works to 1800
There are some alembics of glass, blown in such a manner by the
workmen, that the body and head form but one continued piece. As these
alembics do not stand in need of having their several pieces luted
together, they are very useful on some occasions, when such exceeding
subtile vapours rise as are capable of transpiring through lutes. The
head must have an aperture at the top, provided with a short tube,
through which, by means of a funnel with a long pipe, the matter to be
distilled may be introduced into the cucurbit. This is to be exactly
closed with a glass stopple, the surface whereof must be made to fit
the inside of the tube in every point, by rubbing those two pieces
well together with emery.
Another sort of alembic hath also been invented, which may be used
with advantage when _Cohobation_ is required; that is, when the liquor
obtained by distillation is to be returned upon the matter in the
cucurbit; and especially when it is intended that this cohobation
shall be repeated a great number of times. The vessel we are speaking
of is constructed exactly in the same manner as that last described;
except that its beak, instead of being in a straight line, as in the
other alembics, forms a circular arch, and re-enters the cavity of the
cucurbit, in order to convey back again the liquor collected in the
head. This instrument hath commonly two beaks opposite to each other,
both turned in this manner, and is called a _Pelican_: it saves the
artist the trouble of frequently unluting and reluting his vessels, as
well as the loss of a great many vapours.
There are certain substances which in distillation afford matters in
a concrete form, or rise wholly in the form of a very light powder,
called _Flowers_. When such substances are to be distilled, the
cucurbit which contains them is covered with a head without a nose,
which is named a _Blind-head_.
When the flowers rise in great quantities and very high, a number of
heads is employed to collect them; or rather a number of a kind of
pots, consisting of a body only without any bottom, which fitting one
into the other form a canal, that may be lengthened or shortened at
pleasure, according as the flowers to be sublimed are more or less
volatile. The last of the heads, which terminates the canal, is quite
close at one end, and makes a true blind-head. These vessels are called
_Aludels_; they are usually of earthen or stone ware.
All the vessels above-mentioned are fit only for distilling such light
volatile matters as can be easily raised and brought over; such as
phlegm, essential oils, fragrant waters, acid oily spirits, volatile
alkalis, _&c._ But when the point is to procure by distillation
principles that are much less volatile, and incapable of rising high,
such as the thick fetid oils, the vitriolic, the nitrous, and the
marine acids, _&c._ we are under a necessity of having recourse to
other vessels, and another manner of distilling.
Public-domain text, read in full here on John Shaqi.
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