Elements of the Theory and Practice of Chymistry, 5th ed.Macquer, Pierre Joseph
History
Elements of the Theory and Practice of Chymistry, 5th ed.
Macquer, Pierre Joseph
Chemistry -- Early works to 1800
Fifthly, to terminate the furnace above, there must be a pyramid formed
of the same materials with the furnace, hollow, quadrangular, three
inches high on a base of seven inches, which base must exactly fit
the upper opening of the furnace: the top of this pyramidal cover must
end in a tube of three inches in diameter and two in heighth, which
must be almost cylindrical, and yet a little inclining to the conical
form. This tube serves, as in the furnaces already described, to carry
the conical funnel, which is fitted to the upper part when a fire of
extraordinary activity is wanted.
The furnace thus constructed is fit to serve all the purposes for
which it is designed: yet before it can be used another piece must be
provided, which, though it does not properly belong to the furnace, is
nevertheless necessary in all the operations performed by it; and that
is a piece contrived to contain the cupels, or other vessels which are
to be exposed to the fire in this furnace. It is called a Muffle, and
is made in the following manner.
On an oblong square, of four inches in breadth, and six or seven in
length, a concave semi-cylinder is erected, in the form of a vault,
which makes a semi-circular canal, open at both ends. One of these
is almost entirely closed, except that near the bottom two small
semi-circular holes are left. In each of its sides likewise two such
holes are made, and the other end is left quite open.
The Muffle is intended to bear and communicate the fiercest heat; and
therefore it must be made thin, and of an earth that will resist the
violence of fire, such as that of which crucibles are made. The Muffle
being thus constructed, and then well baked, is fit for use.
Public-domain text, read in full here on John Shaqi.
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