Elements of the Theory and Practice of Chymistry, 5th ed.Macquer, Pierre Joseph
History
Elements of the Theory and Practice of Chymistry, 5th ed.
Macquer, Pierre Joseph
Chemistry -- Early works to 1800
When it is to be used it must be put into the furnace by the upper
opening, and set upon two iron bars, introduced through the holes
made for that purpose below the door of the fire-place. The Muffle
must be placed on these bars in the fire-place in such a manner that
its open end shall stand next to, and directly against the door of
the fire-place, and may be joined to it with lute. Then the cupels
are ranged in it, and the furnace is filled up, to the heighth of two
or three inches above the Muffle, with small coals not bigger than
a walnut, to the end that they may lie close round the Muffle, and
procure it an equal heat on every side. The chief use of the Muffle
is to prevent the coals and ashes from falling into the cupels, which
would be very prejudicial to the operations carrying on in them:
for the lead would not vitrify as it ought, because the immediate
contact of the coals would continually restore its phlogiston; or
else the glass of lead, which ought to penetrate and pass through the
cupels, would be rendered incapable of so doing; because the ashes
mixing therewith would give it such a consistence and tenacity as
would destroy that property, or at least considerably lessen it. The
openings, therefore, which are left in the lower part of the Muffle,
should not be so high as to admit coals or ashes to get into the
cupels; the use of them is to procure an easier passage for the heat
and the air to those vessels. The Muffle is left quite open in its
fore-part, that the operator may be at liberty to examine what passes
in the cupels, to stir their contents, to remove them from one place
to another, to convey new matters into them, &c. and also to promote
the free access of the air, which must concur with the fire towards the
evaporation necessary to the vitrification of lead; which air, if fresh
were not often enough admitted, would be incapable of producing that
effect; because it would soon be loaded with such a quantity of vapours
that it could not take up any more.
The government of the fire in this furnace is founded on the general
principles above laid down for all furnaces. Yet as there are some
little differences, and as it is very essential to the success of the
operations for which this furnace is intended, that the artist should
be absolutely master of his degree of heat, we shall in few words shew
how that may be raised or lowered.
When the furnace is filled with coals and kindled, if the door of the
ash-hole be set wide open, and that of the fire-place shut very close,
the force of the fire is increased; and if, moreover, the pyramidal
cover be put on the top, and the conical funnel added to it, the fire
will become still more fierce.
Public-domain text, read in full here on John Shaqi.
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