Elements of the Theory and Practice of Chymistry, 5th ed.Macquer, Pierre Joseph
History
Elements of the Theory and Practice of Chymistry, 5th ed.
Macquer, Pierre Joseph
Chemistry -- Early works to 1800
Seeing the matters contained in this furnace are encompassed with fire
on all sides, except in the fore-part opposite to the door of the
fire-place, and as there are occasions which require that the force
of the fire should be applied to this part also, an iron box, of the
shape and size of the door, hath been contrived to answer that purpose.
This box is filled with lighted coals, and applied immediately to the
door-place, by which means the heat there is considerably augmented.
This help may be made use of at the beginning of the operation, in
order to accelerate it, and bring the heat sooner to the desired
degree; or in case a very fierce heat be required; or at a time when
the air being hot and moist will not make the fire burn with the
necessary vigour.
The heat may be lessened by removing the iron box, and shutting the
door of the fire-place quite close. It may be still further and
gradually diminished, by taking off the conical funnel from the top; by
shutting the door of the fire-place with one of its plates only, that
which has the least, or that which has the greatest aperture in it; by
taking off the pyramidal cover; by shutting the ash-hole door wholly or
in part; and, lastly, by setting the door of the fire-place wide open:
but, in this last case, the cold air penetrates into the cavity of the
Muffle, and refrigerates the cupels more than is almost ever necessary.
If it be observed, during the operation, that the Muffle grows cold
in any particular part, it is a sign there is a vacuity left by the
coals in that place: in this case an iron wire must be thrust into the
furnace, through the hole which is over the door of the fire-place, and
the coals stirred therewith, so as to make them fall into their places
and fill up the vacant interstices.
It is proper to observe, that, besides what has been said concerning
the ways of increasing the activity of the fire in the cupelling
furnace, several other causes also may concur to procure to the matters
contained in the Muffle a greater degree of heat: for example, the
smaller the Muffle is, the wider and more numerous the holes in it are;
the nearer to its bottom, or further end, the cupels are placed, the
more will the matters therein contained be affected with heat.
Besides the operations to be performed by the cupel, this furnace
is very useful, and even necessary, for many chymical experiments;
such, for instance, as those relating to sundry vitrifications and
enamelling. As it is pretty low, the best way is to place it, when it
is to be used, on a base of brick-work that may raise it to a level
with the operator's hand.
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Elsewhere in the archive
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account