Elements of the Theory and Practice of Chymistry, 5th ed.Macquer, Pierre Joseph
History
Elements of the Theory and Practice of Chymistry, 5th ed.
Macquer, Pierre Joseph
Chemistry -- Early works to 1800
A Lamp-furnace is exceeding useful for all operations that require
only a moderate, but long-continued, degree of heat. The furnace for
working with a lamp-heat is very simple: it consists only of a hollow
cylinder, from fifteen to eighteen inches high, and five or six in
diameter, having at its bottom an aperture large enough for a lamp to
be introduced and withdrawn with ease. The lamp must have three or four
wicks, to the end that by lighting more or fewer of them a greater
or less degree of heat may be produced. The body of the furnace must
moreover have several small holes in it, in order to supply the flame
of the lamp with air enough to keep it alive.
On the top of this furnace stands a bason five or six inches deep,
which ought to fill the cavity of the cylinder exactly, and to be
supported at its circumference by a rim which may entirely cover and
close the furnace: the use of this bason is to contain the sand through
which the lamp-heat is usually conveyed.
Besides this, there must be a kind of cover or dome made of the same
material with the furnace, and of the same diameter with the sand-bath,
without any other opening than a hole, nearly circular, cut in its
lower extremity. This dome is a sort of reverberatory, which serves
to confine the heat and direct it towards the body of the retort; for
it is used only when something is to be distilled in a vessel of this
fashion; and then the hole at its bottom serves for a passage to the
neck of the retort. This dome should have an ear or handle, for the
conveniency of putting it on and taking it off with ease.
_Of Lutes._
Chymical vessels, especially such as are made of glass, and the earthen
vessels commonly called stone-ware, are very subject to break when
exposed to sudden heat or cold: whence it comes, that they often crack
when they begin to heat, and also when being very hot they happen to be
cooled, either by fresh coals thrown into the furnace, or by the access
of cold air. There is no way to prevent the former of these accidents,
but by taking the pains to warm your vessel very slowly, and by almost
insensible degrees. The second may be avoided by coating the body of
the vessel with a paste or lute, which being dried will defend it
against the attacks of cold.
The fittest stuff for coating vessels is a composition of fat earth,
Windsor-loam, fine sand, filings of iron, or powdered glass, and
chopped cow's hair, mixed and made into a paste with water. This lute
serves also to defend glass vessels against the violence of the fire,
and to prevent their melting easily.
In almost all distillations it is of great consequence, as hath been
said, that the neck of the distilling vessel be exactly joined with
that of the receiver into which it is introduced, in order to prevent
the vapours from escaping into the air and so being lost: and this
junction is effected by means of a lute.
Public-domain text, read in full here on John Shaqi.
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