Elements of the Theory and Practice of Chymistry, 5th ed.Macquer, Pierre Joseph
History
Elements of the Theory and Practice of Chymistry, 5th ed.
Macquer, Pierre Joseph
Chemistry -- Early works to 1800
"If the air rushes out with too much rapidity, and with a hissing
noise, the door of the ash-hole must be entirely shut, in order to
slacken the fire. If it do not strike pretty smartly against the
hand, that door must be opened wider, and large coals thrown into the
fire-place to quicken the fire immediately.
"The operation usually lasts four and twenty hours; and the following
signs shew that it will succeed, provided the retort resist the fire.
"You must begin the operation with putting some unlighted charcoal in
the ash-hole, and a little lighted charcoal at the door thereof, in
order to warm the retort very slowly. When the whole is kindled, push
it into the ash-hole, and close the door thereof with a tile. This
moderate heat brings over the phlegm of the mixture. The same degree of
fire must be kept up four hours, after which some coals may be laid on
the grate of the fire-place, which the fire underneath will kindle by
degrees. With this second heat brought nearer the retort, the ballon
grows warm, and is filled with white vapours, which have the smell of
fetid oil. In four hours after, this vessel will grow cool and clear;
and then you must open the door of the ash-hole one inch, throw fresh
coals into the fire-place every three minutes, and every time shut the
door of it, lest the cold air from without should strike against the
bottom of the retort and crack it.
"When the fire has been kept up to this degree for about two hours, the
inside of the ballon begins to be netted over with a volatile salt of a
singular nature, which cannot be driven up but by a very violent fire,
and which smells pretty strong of peach-kernels. Care must be taken
that this concrete salt do not stop the little hole in the ballon: for
in that case it would burst, the retort being then red-hot, and the
air exceedingly rarefied. The water in the ballon, being heated by the
vicinity of the furnace, exhales vapours which dissolve this sprigged
salt, and the ballon clears up in half an hour after it has ceased
rising.
"In about three hours from the first appearance of this salt, the
ballon is again filled with new vapours, which smell like Sal Ammoniac
thrown upon burning coals. They condense on the sides of the receiver
into a salt which is not branched like the former, but appears in long
perpendicular streaks, which the vapours of the water do not dissolve.
These white vapours are the fore-runners of the Phosphorus, and a
little before they cease to rise they lose their first smell of Sal
Ammoniac, and acquire the odour of garlic.
Public-domain text, read in full here on John Shaqi.
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