Elements of the Theory and Practice of Chymistry, 5th ed.Macquer, Pierre Joseph
History
Elements of the Theory and Practice of Chymistry, 5th ed.
Macquer, Pierre Joseph
Chemistry -- Early works to 1800
If you make use of the Nitrous Acid, you must cease adding more filings
when the liquor, after standing still some moments, becomes turbid;
for, when this Acid is impregnated with Iron to a certain degree, it
lets fall some of that which it had dissolved, and becomes capable of
taking up fresh filings. Thus, by constantly adding new supplies of
Iron, this Acid may be made to dissolve a much greater quantity thereof
than is necessary to saturate it entirely. This solution is of a russet
colour, and doth not crystallize.
If the weather be not extremely cold, and the Acids have a proper
degree of strength, the sand-bath is unnecessary, as the dissolution
will succeed very well without it.
Iron dissolved by Acids may be separated therefrom, like all other
metallic substances in the same circumstances, either by the action
of fire, which carries off the Acid and leaves the Martial Earth, or
by the interposition of substances which have a greater affinity than
metallic substances have with Acids; that is, by Absorbent Earths
and Alkaline Salts. By whatever means you separate Iron from an Acid
solvent, it constantly appears, after the separation, in the form of
a yellowish red powder; because it is then deprived of most of the
phlogiston to which it owed its metalline form; whence it is reasonable
to think, that this is the proper colour of Martial earth.
All these precipitates of Iron are true Saffrons of Mars, which,
as well as those prepared by calcination, are so much the further
removed from the nature of a metal, the more they are deprived of
their phlogiston. Thence it comes that they are more or less soluble
by Acids, and more or less attracted by the magnet: as no ferruginous
earth, perfectly deprived of all inflammable matter, is at all
attracted by the magnet, or soluble by Acids.
CHAP. V.
_Of_ TIN.
PROCESS I.
_To extract Tin from its Ore._
Break your Tin ore into a coarse powder, and by washing carefully
separate from it all the heterogeneous matters, and ores of a different
kind, that may be mixed therewith. Then dry it, and roast it in a
strong degree of fire, till no more Arsenical vapour rise from it. When
the ore is roasted, reduce it to a fine powder, and mix it thoroughly
with twice its weight of the black flux well dried, a fourth part of
its weight of clean iron filings, together with as much borax and
pitch; put the mixture into a crucible; over all put Sea-salt to the
thickness of four fingers, and cover the crucible close.
Set the crucible thus prepared in a melting furnace: apply at first a
moderate and slow degree of fire, till the flame of the pitch, which
will escape through the joint of the cover, disappear entirely. Then
suddenly raise your fire, and urge it with rapidity to the degree
necessary for melting the whole mixture. As soon as the whole is in
fusion take the crucible out of the furnace, and separate the Regulus
from the scoria.
_OBSERVATIONS._
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Elsewhere in the archive
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account