Non-technical chats on iron and steel, and their application to modern industrySpring, La Verne W. (La Verne Ward)
History
Non-technical chats on iron and steel, and their application to modern industry
Spring, La Verne W. (La Verne Ward)
Iron; Steel
The exactly weighed portions are put into clean, numbered beakers, which
are small pieces of high grade glassware that will stand sudden changes
of heat and cold. Some of these portions are dissolved in nitric acid,
some in hydrochloric acid, others in combinations of acids. In each case
the drillings go into solution in the acids, and after various
treatments of boiling, evaporating, filtering, etc., well known to those
of the chemical profession, the desired results are obtained. In some
cases it is by actually weighing a constituent which has been filtered
out and burned to ash of a constant known composition, in others it is
by comparison of color with standards of known composition, and
sometimes it is by other means.
[Illustration:
FILTERING SILICONS
After evaporating the excess acid, baking dry, cooling, and
redissolving in weaker acid, the silicon compound formed may be
filtered out. The iron and other soluble constituents, now in
solution, pass through the filter, which is of pure, porous,
unglazed paper.
]
In all of this analytical work the chemist must take care to lose not
one drop of the solution or one grain of the ash from the burned
“precipitate,” as the “filtered out” constituent is called.
The pig iron is always bought upon guarantee that it will contain a
certain percentage of silicon—the element which in cast iron is known as
a “softener.” But this is not the only thing necessary in the iron that
is purchased. It must also show proper specified quantities of
manganese, phosphorus and carbon, which also are very desirable elements
in iron castings, and as little of that undesirable element, sulphur, as
possible. Therefore they pay in proportion to the content of silicon,
manganese, phosphorus, and carbon—and penalize the seller for sulphur.
[Illustration:
“BURNING OFF” THE SILICONS
The paper and contents, in a little crucible, are placed in a red-hot
muffle furnace. The paper is such pure cellulose that it leaves no
weighable ash. That which remains after burning is silicon oxide,
which is a perfectly white, fine sand. This is very carefully
weighed. (Ordinary sand is silicon oxide usually slightly colored
with iron.)
]
The laboratory holds copies of the contracts upon which these materials
were bought. If, upon comparison, the analysis obtained complies with
the terms of the contract, an O. K. unloading slip is made out and the
receiving department is given directions into what raw-material bin in
the receiver building it shall be unloaded. If not fully up to the
standard called for in the contract, the purchasing department is
notified and the car is either rejected or accepted upon some proper
terms of adjustment if it can be used without detriment to the product
in which it is to be utilized.
Public-domain text, read in full here on John Shaqi.
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