Notes and Queries, Number 225, February 18, 1854: A Medium of Inter-communication for Literary Men, Artists, Antiquaries, Genealogists, etc. — John Shaqi
Notes and Queries, Number 225, February 18, 1854: A Medium of Inter-communication for Literary Men, Artists, Antiquaries, Genealogists, etc.Various
History
Notes and Queries, Number 225, February 18, 1854: A Medium of Inter-communication for Literary Men, Artists, Antiquaries, Genealogists, etc.
Various
Questions and answers -- Periodicals
I do not pretend to make a collodion which is different in its ingredients
from that compounded by others. The only thing is that I am anxious to
define the best proportions for making it, and to give a formula which even
the most unpractised operator may work by. First, to produce the collodion
I always use the soluble paper prepared according to the method indicated
by MR. CROOKES, and to which I adverted in "N. & Q.," Vol. viii., p. 252.
Take of colourless nitric acid of 1.50, and sulphuric acid of 1.60, equal
quantities by measure, and mix them; then plunge into the mixture as much
of the best Swedish filtering paper (Papier Joseph is also very good) as
the liquid will cover; it must be placed in it a single piece at a time.
Cover the basin, and let it remain a night, or at least some hours. Then
pour off the liquid, and wash the paper till its washings cease to taste
the least acid, or to redden litmus paper. Then dry it. Of this paper I
take 180 grains to one pint of ether, and having placed them together, I
add alcohol drop by drop, till the ether begins to dissolve the paper,
which will be denoted by the paper becoming quite transparent. I have
rather increased the quantity of paper to be added, as the after treatment
rather thins the collodion. This, when shaken up and completely dissolved,
forms the collodion. To sensitize I use two preparations, one prepared with
potassium, the other with ammonium compounds; and, contrary to what many
operators find the case, I find that the potassium gives the most rapid
results. To prepare the potassium sensitizer, I take two bottles of, we
will suppose, 6 oz. each; into one of these I put about half an ounce of
iodide of potassium in fine powder, and into the other an equal quantity of
bromide of potassium, also pounded; we will call these No. 1. and No. 2. I
fill the bottle No. 1. with absolute alcohol, taking great care that there
is no oxide of amyle in it, as that seriously interferes with the action of
the collodion. After leaving the alcohol in No. 1. for two hours, or
thereabouts, constantly shaking it, let it settle, and then quite clear
decant it off into No. 2., where leave it again, with constant shaking, for
two hours, and when settled decant the clear liquid into a third bottle for
use. The oxide of amyle may be detected by taking a portion of the alcohol
between the palms of the hands, and rubbing them together, till the alcohol
evaporates, after which, should oxide of amyle be present, it will easily
be detected by its smell, which is not unlike that exhaled by a diseased
potato. Of the liquid prepared, take one part to add to every three parts
of collodion. The next, or ammonium sensitizer, is made as follows. Take
Absolute alcohol 10 oz.
Iodide of ammon. 100 grs.
Bromide of ammon. 25 grs.
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