Chemical apparatus; Electroplating; Glass blowing and working; Glass coatings; Glass grinding and polishing; Lampwork; Mirrors
For many purposes the small dimensions of the flame render it very
convenient, and the high temperature which can be attained at exact
spots enables glass to be fused together after a certain amount of
mixing, which is an enormous advantage in fusing lead glass on to hard
glass. The lead glass should not be heated hot enough to burn, but,
short of this, the more fluid it is the better for joints between
dissimilar samples.
It will be noticed that the blow-pipe can be rotated about a vertical
axis so as to throw the flame in various directions. This is often
indispensable.
Sec. 15. In general the oxygen flame does not require to be delivered
under so high a pressure as for the production of a lime light. In
England, I presume, most experimenters will obtain their oxygen ready
prepared in bottles, and will not have to undergo the annoyance of
filling a bag. If, however, a bag is used, and it has some advantages
(the valves of bottles being generally stiff), I find that a pressure
produced by placing about two hundredweight (conveniently divided into
four fifty-six pound weights) on bags measuring 3' x 2'6" x 2' (at the
thicker end) does very well. To fill such a bag with oxygen, about
700 grms of potassium chlorate is required.
If the experimenter desires to keep his bag in good order, he must
purify his oxygen by washing it with a solution of caustic soda, and
then passing it through a "tower" of potash or soda in sticks, and,
finally, through a calcium chloride tower. This purifying apparatus
should be permanently set up on a board, so that it may be carried
about by the attendant to wherever it is required. Oxygen thus
purified does not seem to injure a good bag--at least during the
first six or seven years:
In order to reduce the annoyance of preparing oxygen, the use of the
usual thin copper conical bottle should be avoided. The makers of
steel gas bottles provide retorts of wrought iron or steel for
oxygen-making, and these do very well. They have the incidental
advantage of being strong enough to resist the attacks of a servant
when a spent charge is being removed.
The form of retort referred to is merely a large tube, closed at one
end, and with a screw coupling at the other; the dimensions may be
conveniently about 5 inches by 10. The screw threads should be filled
with fireclay (as recommended by Faraday) before the joint is screwed
up. Before purchasing a bottle the experimenter will do well to
remember that unless it is of sufficiently small diameter to go into
his largest vice, he will be inconvenienced in screwing the top on and
off. Why these affairs are not made with union joints, as they should
be, is a question which will perhaps be answered when we learn why
cork borers are still generally made of brass, though steel tube has
long been available.
Fig. 4.
Public-domain text, read in full here on John Shaqi.
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