Perfumes and their preparation : $b Containing complete directions for making handkerchief perfumes, smelling-salts, sachets, fumigating pastils; preparations for the care of the skin, the mouth, the hair; cosmetics, hair dyes, and other toilet articlesAskinson, George William
Science
Perfumes and their preparation : $b Containing complete directions for making handkerchief perfumes, smelling-salts, sachets, fumigating pastils; preparations for the care of the skin, the mouth, the hair; cosmetics, hair dyes, and other toilet articles
Askinson, George William
Cosmetics; Perfumes
About four pounds of benzoin B of best quality is broken into small
pieces and placed in a small copper boiler K (Fig. 3); over its entire
surface is pasted white blotting paper L, and to this is pasted a cone
of strong paper which must surround the edge of the boiler. The cone
ends above in a paper tube R, about five feet long and an inch wide.
The copper boiler is placed in a large clay pot T (a flower pot) and
surrounded on all sides with fine sand. The clay pot is heated from
without by a charcoal fire. After the pot has remained about half an
hour on the fire, the latter is fanned to its utmost and kept at this
point for thirty minutes. The heat volatilizes the benzoic acid, the
above-mentioned essential oil, and some tarry substances of a brown
color. The latter are arrested by the filter paper, while the benzoic
acid is deposited on the cone and in the tube, in the form of delicate
glossy needles which are very fragrant owing to the essential oil.
The largest yield of benzoic acid is obtained when the temperature is
raised very gradually, until finally nothing remains in the copper
boiler but a brown, almost carbonized mass of a blistered appearance.
[Illustration: FIG. 3.]
BORAX (SODII BORAS)
is used in some preparations. Borax forms colorless crystals which
slightly effloresce in dry air and hence must be preserved in tightly
closed vessels. Reddish tinted crystals are contaminated with oxide of
iron and should be rejected.
PERMANGANATE OF POTASSIUM (POTASSI PERMANGANAS)
is a salt formed by fusing a mixture of manganese dioxide, potassa, and
potassium chlorate, extracting the product with water, and evaporating
the solution to crystallization; the salt is obtained in small dark
violet, almost black crystals which dissolve in sixteen parts of water
to which they impart a beautiful violet color. By contact with organic
substances, or others easily oxidized, the solution changes its color
into green and finally is decolorized, precipitating a brown powder.
Owing to this change of color the salt has been called chameleon
mineral. As its preparation requires considerable dexterity, it is
preferable to buy it from reputable houses, rather than to make it. It
is used in the manufacture of mouth washes and hair dyes. The solution
of the salt causes brown stains on linen and the skin; they can be
removed only if the spots are immediately washed with hydrochloric,
oxalic, sulphuric, or another acid.
ACETIC ACID (ACIDUM ACETICUM).
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