=8. Mixed Fertilizers.=—In fertilizing materials in bulk, the first
requisite is that they shall be thoroughly mixed so that a given volume
of the material may represent, practically, definite quantities of the
materials sampled. The finer the material is, in the original state,
and the more thoroughly it has been mixed, the better the sample will
be. If the sample be already in sacks it will be sufficient to take
portions by means of the ordinary trier, such as is used for sampling
sugar and other substances. This consists of a long metal implement
such as would be formed by a longitudinal section of a tube. The end
is pointed and suited for penetrating into the sack and the materials
contained therein. On withdrawing it, the semi-circular concavity is
found filled with the material sampled. Samples in this way should
be taken from various parts of the sack and these samples well mixed
together and a subsample of the amount necessary to be taken to the
laboratory can then be obtained.
=9. Method of the French Experiment Stations.=—In the method employed
by the French Experiment Stations it is directed that in no case should
stones or other foreign particles be removed from the fertilizer
sampled, but they should enter into the sample taken in, as nearly as
possible, the same proportions as they exist in the whole mass.
In the case of stones or other solid masses which are to be sampled, as
many samples as possible should be taken from all parts of the heap and
these should be reduced to a coarse powder, thoroughly mixed together
and sampled.
In case the material is in the form of a paste, if it is homogeneous,
it will be sufficient to mix it well and take the sample directly; but
in case there is a tendency for the pasty mass to separate into two
parts, of which the one is a liquid and the other, more of a solid
consistence, it may be well to take samples from each in case they can
not be thoroughly incorporated by stirring.
=10. Method of the French Association of Sugar Chemists.=—The method
adopted by the French sugar chemists directs that the sample should be
taken from the fertilizer in bulk or from a portion used for industrial
purposes.[4] The sample for analysis is to be taken from the above
sample after it has been sent to the laboratory. The method of taking
should be varied according to the condition of the substances to be
analyzed.
The large sample selected from the goods delivered to commerce having
been delivered at the laboratory, the analytical sample is taken as
follows:
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