=129. Digestion Apparatus for Reverted Phosphates.=—The digestion
apparatus used by Huston consists of two wheels twenty-five centimeters
in diameter, mounted on the same axis, having a clear space of four and
one-half centimeters between them.[118] In the periphery of each wheel
are cut twelve notches, which are to receive the posts bearing the
rings through which the necks of the flasks pass. The posts are held in
place by nuts which are screwed down on the faces of the wheel. Should
it become necessary to take the apparatus apart, it is only necessary
to loosen the nuts and the set screw holding one wheel to the shaft and
all the parts can at once be removed. The posts extend ten centimeters
beyond the face of the wheels, and the rings are four centimeters in
internal diameter. Perforated plates, bearing a cross-bar, and held in
place by strong spiral springs attached to the plate and the base of
the posts, serve to hold the flasks in place. Each plate has a number
stenciled through it for convenience in identifying the flasks when it
is time to remove them. Attached to the outside of each post, close
to the outer end, is a heavy wire which passes entirely around the
apparatus, serving to keep the plates in place after they are removed
from the flasks.
The apparatus is mounted on a substantial framework, thirty-six
centimeters high and thirty centimeters wide at the base. The space
in which the wheel revolves is fourteen centimeters wide. The base
bars connecting the two sides are extended seven centimeters beyond
one side, and serve for the attachment of lateral bracing. At the top
of the framework, at one side, is attached a heavy bar forty-five
centimeters long, which serves to carry the cog gearing which transmits
the power. The upright shaft carries a cone pulley to provide for
varying the speed. The usual speed is two revolutions a minute for the
wheel carrying the flasks. The entire apparatus is made of brass. The
details of construction are shown in Fig. 8. Round-bottomed flasks are
used, and rubber stoppers are held in place by tying or by a special
clamp shown at the lower right-hand of the figure.
When high temperatures are used, the plates and flasks are handled by
the hooks shown at the left and right-hand upper corners of the figure.
When any other than room temperature is desired, the whole apparatus is
immersed in water contained in the large galvanized tank forming the
back-ground of the figures. The tank is seventy-five centimeters long,
seventy-five centimeters high, and thirty centimeters wide. At one end,
near the top, is an extension to provide space for heating the fluid in
the flasks before introducing the solid in such cases as may be desired.
The apparatus is held in place by angle irons soldered to the bottom
of the tank and a brace resting against the upright bar bearing the
gear-wheels.
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