=236. Estimation of Dry Substance, Polarization and Apparent Purity for
Factory Control.=—For technical purposes the methods of determining
the above factors, proposed by Weisberg and applicable to concentrated
sirups, massecuites, and molasses, may be used.[193] Five times the half
normal quantity of the material, _viz._, 65.12 grams, are placed in a
quarter liter flask, dissolved in water and the flask filled to the
mark. In the well shaken mixture, which is allowed to stand long enough
to be free of air, the degree brix is estimated by an accurate spindle.
For example, in the case of molasses, let the number obtained be 18.8.
Fifty cubic centimeters of the solution are poured into a 100 cubic
centimeter flask, the proper quantity of lead subacetate added, the
flask filled to the mark with water, its contents filtered, and the
filtrate polarized in a 200 millimeter tube. Let the number obtained
on polarization be 22°.1. This number may be used in two ways. If
it be multiplied by two the polarization of the original sample is
obtained; in this case, _viz._, 44°.2. In the second place, if 44.2 be
multiplied by 0.26048 and this product divided by the specific gravity
corresponding to 18°.8. _viz._, 1.078, the quotient 10.68 is secured
representing the polarization or per cent of sugar contained in the
solution of which the degree brix was 18.8°. From the numbers 18.8 and
10.68 the apparent purity of the solution, 56.8, is calculated, _viz._,
10.68 × 100 ÷ by 18.8. The original product as calculated above gives a
polarization of 44.2 and this number multiplied by 100 and divided by
56.8 gives 77.8, or the apparent percentage of dry matter. The original
sample of molasses, therefore, had the following composition:
Degree brix (total solids) 77.8 per cent.
Sucrose 44.2 ”
Solids, not sucrose 33.6 ”
Apparent purity 56.8 ”
It is seen from the above that with a single weighing and a single
polarization, and within from ten to fifteen minutes, all needful
data in respect of the proper treatment of molasses for the practical
control and direction of a factory can be obtained.
In case a laurent polariscope is used, five times the normal weight,
_viz._, eighty-one grams of the raw material are used and the process
conducted as above.
SUCROSE, DEXTROSE, INVERT SUGAR, LEVULOSE, MALTOSE, RAFFINOSE, DEXTRIN
AND LACTOSE IN MIXTURES.
=237. Occurrence.=—Sucrose and invert sugar are found together in many
commercial products, especially in raw sugars and molasses made from
sugar cane, and in these products sucrose is usually predominant. They
also form the principal saccharine contents of honey, the invert sugar,
in this case, being the chief ingredient.
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