In the figure the thermometer and aperture for introducing dry air or
an inert gas are shown in the movable end disk, but they would be more
conveniently placed in the fixed end. The oven is heated below by a gas
burner, which conveniently should be as long as the oven. The heat is
not allowed to strike the brass cylinder directly, but the latter is
protected by a piece of asbestos paper.
The temperature inside of the oven can be easily kept practically
constant by means of a gas regulator, not shown in the figure, or
by a little attention to the lamp. For a vacuum of twenty inches a
temperature of about 80° should be maintained. When the vacuum is more
complete a lower temperature can be employed. This apparatus is simple
in construction, strong, cheap, and highly satisfactory in use.
=21. Drying in Hydrogen.=—In some of the processes of agricultural
analysis it becomes important to dry the sample in hydrogen or other
inert gas. This may be accomplished by introducing the dry gas desired
into some form of the apparatus already described. The drying may
either be accomplished in an atmosphere of hydrogen practically at rest
or in a more limited quantity of the gas in motion. The latter method
is to be preferred by reason of its greater rapidity. The analyst
has at his command many forms of apparatus designed for the purpose
mentioned above. It will be sufficient here to describe only two,
devised particularly for agricultural purposes.
The first one of these, designed by the author, was intended especially
for drying the samples of fodders for analysis according to the methods
of the Association of Agricultural Chemists.[8]
[Illustration: FIGURE 11. APPARATUS FOR DRYING IN A CURRENT OF
HYDROGEN.]
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