Pumice stone, on account of its great porosity, is also an excellent
medium for the distribution of a viscous liquid in aiding the process
of desiccation. The method has been worked out in great detail in
this laboratory by Carr and Sanborn,[14] and most excellent results
obtained. Round aluminum dishes two centimeters high and from eight to
ten centimeters in diameter are conveniently used for this process.
The pumice stone is dried and broken into fragments the size of a pea
before use.
=27. General Principles of Drying Samples.=—It would be a needless
waste of space to go into further details of devices for desiccation. A
sufficient number has been given to fully illustrate all the principles
involved. In general, it may be said that drying in the open air at a
temperature not exceeding that of boiling water can be safely practiced
with the majority of samples. For instance, we have found practically
no change in this laboratory in the composition of cereals dried in
the air and in an inert gas. The desiccation should in all cases be
accomplished as speedily as possible. To this end the atmosphere in
contact with the sample should be dry and kept in motion. An oven
surrounded by boiling water and steam is to be preferred to one heated
by air. Constancy of temperature is quite as important as its degree
and this steadiness is most easily secured by steam at atmospheric
pressure. Where higher temperatures than 100° are desired the steam
must be under pressure, or the boiling-point of the water may be raised
by adding salt or other soluble matters. A bath of paraffin or calcium
chlorid may also be used or a sand or air-bath may be employed. The
analyst must not forget, however, that inorganic matters are prone to
change at temperatures above 100°, even in an inert atmosphere, and
higher temperatures must be used with extreme caution.
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account