=39. Knorr’s Extraction Apparatus.=—The apparatus which has been
chiefly used in this laboratory for the past few years is shown in
the accompanying figure.[18] The principle of the construction of the
apparatus lies in the complete suppression of stoppers and in sealing
the only joint of the device with mercury.
The construction and operation of the apparatus will be understood by a
brief description of its parts.
A is the flask containing the solvent, W a steam bath made by cutting
off the top of a bottle, inverting it and conducting the steam into one
of the tubes shown in the stopper while the condensed water runs out of
the other. The top of the bath is covered with a number of concentric
copper rings, so that the opening may be made of any desirable size. B
represents the condenser, which is a long glass tube on which a number
of bulbs has been blown, and which is attached to the hood for holding
the material to be extracted, as represented at Bʹ, making a solid
glass union. Before joining the tube at Bʹ the rubber stopper which is
to hold it into the outside condenser of B is slipped on, or the rubber
stopper may be cut into its center and slipped over the tube after the
union is made. In case alcohol is to be used for the solvent, requiring
a higher temperature, the flask holding the solvent is placed entirely
within the steam-bath, as represented at Aʹ.
[Illustration: FIGURE 18. KNORR’S EXTRACTION APPARATUS.]
[Illustration: FIGURE 19. EXTRACTION FLASK.]
[Illustration: FIGURE 20. EXTRACTION TUBE.]
[Illustration: FIGURE 21. EXTRACTION SIPHON TUBE.]
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