Pyrometry: A Practical Treatise on the Measurement of High Temperatures — John Shaqi
Pyrometry: A Practical Treatise on the Measurement of High TemperaturesDarling, Charles R. (Charles Robert)
Science
Pyrometry: A Practical Treatise on the Measurement of High Temperatures
Darling, Charles R. (Charles Robert)
Pyrometry
=Standardization by Fixed Points.=—Taking any millivoltmeter
which, with a maximum of 20 millivolts at the terminals, will give a
full scale deflection, the first step is to arrange that the pointer
(or spot of light) shall just remain on the scale at the highest
temperature to be attained by the junction. This may be done by placing
the hot junction in boiling water and noting the deflection obtained,
either in millivolts or equal arbitrary divisions, and also the
temperature of the cold junction. The deflection observed is due to
a difference of temperature (100-_t_) deg. C, where _t_ is the
temperature of the cold junction. If the highest temperature to be
measured is 10 times (100-_t_), the deflection should be rather
less than 1/10 of the scale, and similarly for any other required
temperature limit. If the observed deflection exceed this proportion, a
series resistance should be added until the correct value is obtained.
This resistance is then permanently installed in the circuit for use
with the junction under trial.
Before proceeding further it is necessary to consider whether the
pyrometer is to possess a single cold junction of ascertainable
temperature (as in fig. 6), or whether it will be arranged with two
cold junctions in the head, as in fig. 4. In the former case it is
simpler to prepare a “difference” scale; that is, one which reads
differences of temperature between the hot and cold junctions, from
which the temperature of the hot end may be obtained by adding to the
difference that of the cold junction. In the latter case the cold end
should be kept by artificial means at the temperature likely to be
attained in practice—say 25° C.—a water-bath being suitable for this
purpose. It is advisable to remove the shield of the pyrometer when
standardizing, so as to expose the hot junction, as closer readings can
then be taken.
A number of materials—preferably cheap—of known boiling points or
melting points are then selected from a table of fixed points (page
16) so as to give about six points, distributed fairly evenly over the
scale. As an example, if it were desired to prepare a temperature scale
from 0° to 1000° C., the following might be chosen:—
════════════════════════════════════════════════╤═══════════════════
Substance and Condition. │ Temperature.
────────────────────────────────────────────────┼─────────┬─────────
Water at boiling point │ 100° C. │ 212° F.
Tin at melting point │ 232 │ 449
Zinc at melting point │ 419 │ 786
Antimony at melting point │ 631 │ 1167
Common salt at melting point │ 800 │ 1472
Copper at melting point (covered with graphite) │1084 │ 1983
════════════════════════════════════════════════╧═════════╧═════════
Public-domain text, read in full here on John Shaqi.
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