Scientific American Supplement, No. 299, September 24, 1881 — John Shaqi
Scientific American Supplement, No. 299, September 24, 1881Various
Science
Scientific American Supplement, No. 299, September 24, 1881
Various
Science -- Periodicals
By their arrangement, which is shown in the opposite figure, they form
a mechanical system permitting of the rectification of alcohols at
temperatures as low as -40° or even -50°. They verify experimentally, by
their operation, the theoretical deductions which precede. The boilers,
A, which, in an industrial application, may be more numerous, receive
their supply of spirits from the country distilleries in the vicinity of
the factory. There may even be introduced directly into them _vinasses_,
or washes, that is to say, liquids, such as are obtained by alcoholic
fermentation.
Above the boiler rises a rectifying column composed of superposed plates
inclined one over the other, and surmounted by a tubular condenser,
which serves to effect the retrogression of the first condensation by
means of a current of water supplied by the reservoir placed above.
On leaving this condenser, the vapors which have escaped condensation
pass into the refrigerator, C, where they are totally condensed by a
current of water which goes to the reservoir above.
The first products obtained contain ethers and impure alcohols, which
are collected in the reservoir, E.
When the first products have been thus introduced into the reservoir,
and it is ascertained by tasting that good alcohol is passing over,
the liquid produced is directed into the second boiler, F. The sliding
valve, operated by a screw having a very fine pitch, establishes a
communication between the refrigerator, C, and the second boiler, F. The
office of this valve we shall learn further on. This first rectification
is performed in a vacuum, for a system of metallic pipes connects the
entire apparatus with an air-pump, O. The temperature at which the
liquids shall enter into ebullition in the boilers, A A, may, then, be
regulated in advance.
The operations will be carried on with a more or less complete vacuum,
according to the nature of the products to be rectified. The distiller
will have to be guided in this by practice alone.
The good tasted products are received in boiler No. 2, F, and there the
liquids are submitted to the action of an almost absolute vacuum. As we
have before said, their temperature falls immediately and spontaneously.
The vapors which issue from this liquid contain almost solely pure
alcohol. The other substances, which passed over in the first
distillation, no longer emit vapors at temperatures ranging between -10°
and +5°. Their temperature is shown by a thermometer running into the
boiler, F.
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account