Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant.Thomssen, Edgar George
Science
Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant.
Thomssen, Edgar George
Soap
The committee has also considered the various distillation methods for
the determination of moisture in fats and oils, but since according to
the fundamental principles which it was endeavoring to follow it could
only standardize one method, it was decided that the most desirable one
on the whole was the vacuum-oven method as given. There are cases
wherein a chemist may find it desirable to check a moisture
determination or investigate the moisture content of a fat or oil
further by means of one of the distillation methods.
However, in co-operative work the distillation method in various types
of apparatus has not yielded satisfactory results. The difficulties
appear to be connected with a proper choice of solvent and particularly
with the tendency of drops of water to adhere to various parts of the
glass apparatus instead of passing on to the measuring device. When
working on coconut oil containing a high percentage of free fatty acids,
concordant results could not be obtained by the various members of the
committee when working with identical samples, solvents and apparatus.
On the other hand, the committee found by individual work, co-operative
work and collaborative work by several members of the committee in one
laboratory, that the old, well-known direct heating method (which the
committee has designated the hot plate method) yielded very satisfactory
results on all sorts of fats and oils including emulsions such as butter
and oleomargarine and even on coconut oil samples containing 15 to 20
per cent free fatty acids and 5 to 6 per cent of moisture.
Unfortunately, this method depends altogether on the operator's skill
and while the method may be taught to any person whether a chemist or
not so that he can obtain excellent results with it, it is difficult to
give a sufficiently, complete description of it so that any chemist
anywhere after reading the description could follow it successfully. The
method is undoubtedly worthy of much confidence in careful hands. It is
quick, accurate and reliable. It is probably the best single method for
the determination of moisture in all sorts of samples for routine
laboratory work. On account of this fact the committee desires to
announce its willingness to instruct any person in the proper use of the
method who desires to become acquainted with it and who will visit any
committee member's laboratory.
INSOLUBLE IMPURITIES.
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Elsewhere in the archive
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account