Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant.Thomssen, Edgar George
Science
Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant.
Thomssen, Edgar George
Soap
Much can be learned by one, who through continued acquaintance with
these oils has thoroughly familiarized himself with the indications of a
good or bad oil, by taste, smell, feel and appearance. It is, however,
not well for the manufacturer in purchasing to depend entirely upon
these simpler tests. Since he is interested in the yield of glycerine,
the largest possible yield of soap per pound of soap stock and the
general body and appearance of the finished product, the chemical tests
upon which these depend should be made. Those especially important are
the acid value, percentage unsaponifiable matter and titer test.
A short description of the various oils and fats mentioned is sufficient
for their use in the soap industry.
_Tallow_ is the name given to the fat extracted from the solid fat or
"suet" of cattle, sheep or horses. The quality varies greatly, depending
upon the seasons of the year, the food and age of the animal and the
method of rendering. It comes to the market under the distinction of
edible and inedible, a further distinction being made in commerce as
beef tallow, mutton tallow or horse tallow. The better quality is white
and bleaches whiter upon exposure to air and light, though it usually
has a yellowish tint, a well defined grain and a clean odor. It consists
chiefly of stearin, palmitin and olein. Tallow is by far the most
extensively used and important fat in the making of soap.
In the manufacture of soaps for toilet purposes, it is usually necessary
to produce as white a product as possible. In order to do this it often
is necessary to bleach the tallow before saponification. The method
usually employed is the Fuller's Earth process.
FULLER'S EARTH PROCESS FOR BLEACHING TALLOW.
From one to two tons of tallow are melted out into the bleaching tank.
This tank is jacketed, made of iron and provided with a good agitator
designed to stir up sediment or a coil provided with tangential downward
opening perforations and a draw-off cock at the bottom. The coil is the
far simpler arrangement, more cleanly and less likely to cause trouble.
By this arrangement compressed air which is really essential in the
utilization of the press (see later) is utilized for agitation. A dry
steam coil in an ordinary tank may be employed in place of a jacketed
tank, which lessens the cost of installation.
The tallow in the bleaching tank is heated to 180deg. F. (82deg. C.) and
ten pounds of dry salt per ton of fat used added and thoroughly mixed by
agitation. This addition coagulates any albumen and dehydrates the fat.
The whole mass is allowed to settle over night where possible, or for at
least five hours. Any brine which has separated is drawn off from the
bottom and the temperature of the fat is then raised to 160deg. F.
(71deg. C).
Five per cent. of the weight of the tallow operated upon, of dry
Fuller's earth is now added and the whole mass agitated from twenty to
thirty minutes.
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