Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant. — John Shaqi
Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant.Thomssen, Edgar George
Science
Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant.
Thomssen, Edgar George
Soap
The new bleached fat, containing the Fuller's earth is pumped directly
to a previously heated filter press and the issuing clear oil run
directly to the soap kettle.
One of the difficulties experienced in the process is the heating of the
press to a temperature sufficient to prevent solidification of the fat
without raising the press to too great a temperature. To overcome this
the first plate is heated by wet steam. Air delivered from a blower and
heated by passage through a series of coils raised to a high temperature
by external application of heat (super-heated steam) is then substituted
for the steam. The moisture produced by the condensation of the steam is
vaporized by the hot air and carried on gradually to each succeeding
plate where it again condenses and vaporizes. In this way the small
quantity of water is carried through the entire press, raising its
temperature to 80deg.-100deg. C. This temperature is subsequently
maintained by the passage of hot air. By this method of heating the poor
conductivity of hot air is overcome through the intermediary action of a
liquid vapor and the latent heat of steam is utilized to obtain the
initial rise in temperature. To heat a small press economically where
conditions are such that a large output is not required the entire press
may be encased in a small wooden house which can be heated by steam
coils. The cake in the press is heated for some time after the
filtration is complete to assist drainage. After such treatment the cake
should contain approximately 15 per cent. fat and 25 per cent. water.
The cake is now removed from the press and transferred to a small tank
where it is treated with sufficient caustic soda to convert the fat
content into soap.
Saturated brine is then added to salt out the soap, the Fuller's earth
is allowed to settle to the bottom of the tank and the soap which
solidifies after a short time is skimmed off to be used in a cheap soap
where color is not important. The liquor underneath may also be run off
without disturbing the sediment to be used in graining a similar cheap
soap. The waste Fuller's earth contains about 0.1 to 0.3 per cent. of
fat.
METHOD FOR FURTHER IMPROVEMENT OF COLOR.
A further improvement of the color of the tallow may be obtained by
freeing it from a portion of its free fatty acids, either with or
without previous Fuller's earth bleaching.
To carry out this process the melted fat is allowed to settle and as
much water as possible taken off. The temperature is then raised to 160deg.
F. with dry steam and enough saturated solution of soda ash added to
remove 0.5 per cent. of the free fatty acids, while agitating the mass
thoroughly mechanically or by air. The agitation is continued ten
minutes, the whole allowed to settle for two hours and the foots drawn
off. The soap thus formed entangles a large proportion of the impurities
of the fat.
VEGETABLE OILS.
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