From what has been said of the different foreign substances used for
adulterations of spices and condiments, the necessity of knowing the
structure and formation of the molecules of both principal and foreign
elements which constitute the principal tissues of the particular
plant-parts used for the adulterations is apparent, while in the
chemical examination the principle of proximate analysis must be
understood and applied.
It is also necessary that the analyst should be thoroughly acquainted
with the application of the microscope, to determine the cellular
structure, to make determinations of proximate principles in the
substances under examination, since a mechanical separation by the
microscope is more expeditious and is more at the command of the
majority of persons searching for adulterations. For a mechanical
analysis of food separations, a powerful microscope of good workmanship
is required. It is better if it is supplied with a substance condenser
and Nical prisms for the use of polarized light. Objectives of an inch
and half inch, and, for some starches, one-fifth inch, equivalent focus,
are sufficient. One eye-piece of medium depth, one-fourth to one-sixth,
adjusted at 160 degrees is enough, with plenty of good light. The
analyst should also have plenty of sieves of 40 to 60 meshes to the inch
to be used for separation, which will furnish means of detecting
adulterants and selecting particles for investigation, and will often
reveal the presence of foreign material without further examination,
since many adulterants are not ground so fine as the spices to which
they are added, and by passing the mixtures through the sieves the
coarser particles remaining will be either recognized at once by an
unaided educated eye or with a pocket lens.
In this way, tumeric is readily separated from mustard and yellow corn
meal; mustard hulls and cayenne, from low-grade pepper. Where a pocket
lens is insufficient, the higher power of the microscope is
confirmatory. It is also desirable to be provided with a dissecting
microscope for selecting particles for examination from large masses of
ground spice, and for this a large Zeiss stand, made for that purpose,
is best, but simpler forms, or even a hand lens, will answer the
purpose. For smaller apparatus, a few beakers, watch crystals, stirring
rods, and specimen tubes, with bottles for reagents, will be sufficient,
in addition to the ordinary glass slides and covers for glasses. The
reagents required for chemical analysis (if no great amount is used) are
as follows:
Strong alcohol,
Ammonia,
Chloral-hydrate solution—8 parts to 5 of water,
Glycerine,
Iodine solution—water 15 parts, iodide of potash 20 parts, iodine 5
parts; water distilled.
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