The A B C of Mining: A Handbook for ProspectorsBramble, Charles A.
Science
The A B C of Mining: A Handbook for Prospectors
Bramble, Charles A.
Mining engineering; Prospecting
Carbonates, that is those minerals that contain carbon and oxygen in
addition to the metal, effervesce when brought into contact with
hydrochloric acid. Some sandstones have a small amount of lime
carbonate, and must be tried under the lens, as the bubbles are
microscopic. These tests are extremely useful, but by no means
infallible, owing to so few ores being pure.
When the explorer wishes to know all the constituents of the ore he
has found, he must analyze it. An analysis gives every substance in
the ore. Such examinations may be either by the "dry" or "wet"
methods, though usually the term "analysis" is restricted to the
latter, and "fire assay" is used to describe the former. The wet assay
for silver, lead or mercury is effected as follows:
Drop a little powdered ore in a test tube; add nitric acid; dilute
with 1/8 water; warm gently over the spirit lamp. It may dissolve or
it may not. In the latter case, add four times as much hydrochloric
acid. Should all these attempts fail, a fresh sample must be taken,
and equal parts of sodium carbonate and potassium carbonate added, and
the whole strongly heated in a platinum crucible. The contents, after
cooling, is dissolved in dilute nitric acid.
In any case the assay will now be dissolved, and will be in the
solution. Filter. Pour ten drops into a test tube; add three or four
drops of hydrochloric acid. A precipitate appears. It may be silver,
lead or mercury. If silver, it grows dark violet after exposure to
sunlight, or 30 or 40 drops of ammonia dissolves it in a few moments.
Should it not dissolve, it is lead or mercury. Test for lead by
filtering, and heating some of the precipitate on charcoal before the
blow-pipe. A bead and yellow incrustation indicate lead. Should none
of these things happen, then the metal is mercury. Filter; place in
glass tubes; heat gently, and a mirror of quicksilver will appear on
the sides of the glass.
This is as far as the prospector, without the various reagents and
chemicals that the analyst has always at hand, will be able to go.
More complex treatment must be reserved until a return to
civilization.
CHAPTER III.
BLOW-PIPE TESTS.
[Illustration: BLOW-PIPE.]
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