The Boy's Playbook of Science: Including the Various Manipulations and Arrangements of Chemical and Philosophical Apparatus Required for the Successful Performance of Scientific Experiments in Illustration of the Elementary Branches of Chemistry and Natural PhilosophyPepper, John Henry
Science
The Boy's Playbook of Science: Including the Various Manipulations and Arrangements of Chemical and Philosophical Apparatus Required for the Successful Performance of Scientific Experiments in Illustration of the Elementary Branches of Chemistry and Natural Philosophy
Pepper, John Henry
Science -- Juvenile literature
Another and still more expeditious mode of preparing a little chlorine,
is by placing a small beaker glass, containing half an ounce of
chlorinated lime, usually termed chloride of lime or bleaching powder,
carefully at the bottom of a deep and large beaker glass, and then, by
means of a tube and funnel, conveying to the chloride of lime some
dilute oil of vitriol, composed of half acid and half water;
effervescence immediately occurs from the escape of chlorine gas, and as
it is produced it falls over the sides of the small beaker glass into
the large one, when it may be distinguished by its green colour. If a
little gas be dipped out with a very small beaker glass arranged as a
bucket, and poured into a cylindrical glass containing some dilute
solution of indigo, and shaken therewith, the colour disappears almost
instantaneously; and if a piece of Dutch metal is thrown into the beaker
glass it will take fire if enough chlorine has been generated, or some
very finely-powdered antimony will demonstrate the same result. Thus,
with a few beaker glasses, some chloride of lime, sulphuric acid, a
solution of indigo, and a little Dutch metal, the chief properties of
chlorine may be displayed. (Fig. 132.)
[Illustration: Fig. 132. A A. The large beaker glass. B. The small one,
containing the chloride of lime. C. The tube and funnel down which the
dilute sulphuric acid is poured. D D. Sheet of paper over top of large
glass, with hole in centre to admit the tube. E. The little beaker used
as a bucket.]
_Fourth Experiment._
Into a little platinum spoon place a small pellet of the metal sodium,
and after heating it in the flame of a spirit lamp, introduce the metal
[Page 133] into a bottle of chlorine, when a most intense and brilliant
combustion occurs, throwing out a vivid yellow light, and the heat is
frequently so great that the bottle is cracked. After the combustion,
and when the bottle is cool, it is usually lined with a white powder,
which will be found to taste exactly the same as salt, and, in fact, is
that substance, produced by the combination of chlorine, a virulent
poison, with the metal sodium, which takes fire on contact with a small
quantity of water; and hence the use of salt for the preparation of
chlorine gas when it is required on the large scale.
Parts.
Common salt 4
Black oxide of manganese 1
Sulphuric acid 2
Water 2
_Fifth Experiment._
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