A Practical Handbook on the Distillation of Alcohol from Farm Products — John Shaqi
A Practical Handbook on the Distillation of Alcohol from Farm ProductsWright, F. B. (Frederic B.)
Science
A Practical Handbook on the Distillation of Alcohol from Farm Products
Wright, F. B. (Frederic B.)
Alcohol; Alcohol, Denatured
=Iron vats= have also been used, having a jacketed space around them,
into which hot or cold water may be introduced. As wooden vats are porous
and hence uncleanly they have to be constantly scrubbed and disinfected.
It is advisable to cover the interior with linseed oil, varnish or with a
shellac varnish. The diameter of the coil varies according to the size of
the vat.
=The room= in which the vats are placed should be made as free from
draughts as possible by dispensing with superfluous doors and windows; it
should not be too high and should be enclosed by thick walls in order to
keep in the heat. As uniformity of temperature is highly desirable, a
thermometer should be kept in the room, and there should be stoves for
supplying heat in case it be required. The temperature should be kept
between 64∞ F. and 68∞ F.
Every precaution must be taken to ensure the most absolute cleanliness;
the floors should be swept or washed with water daily, and the vats, as
pointed out above, must be cleaned out as soon as the contents are
removed. For washing the vats, lime-water should be used when the
fermentation has been too energetic or has shown a tendency to become
acid; water acidulated with sulphuric acid is used when the action has
been feeble and the fermented liquor contains a small quantity of
undecomposed sugar. Care must be taken to get rid of carbonic anhydride
formed during the operation. Buckets of lime-water are sometimes placed
about the room for the purpose of absorbing this gas; but the best way of
getting rid of it is to have a number of holes, three or four inches
square, in the floor, through which the gas escapes by reason of its
weight. The dangerous action of this gas and its effects upon animal life
when unmixed with air are too well know to necessitate any further
enforcement of these precautions.
=The beer= obtained by mashing and fermenting consist essentially of
volatile substances, such as water, alcohol, essential oils and a little
acetic acid, and of non-volatile substances, such as cellulose, dextrine,
unaltered sugar and starch, mineral matters, lactic acid, etc.
=The volatile constituents= of the liquor possess widely different
degrees of volatility; the alcohol has the lowest boiling point, water
the next, then acetic acid, and last the essential oils. It will thus be
seen that the separation of the volatile and non-volatile constituents by
evaporation and condensation of the vapors given off is very easily
effected, and that also by the same process, which is termed
_distillation_, the volatile substances may be separated from one
another. As the acetic acid and essential oils are present only in very
small quantities, they will not require much consideration.
The aim of distillation is to separate as completely as possible the
alcohol from the water which dilutes it. Table I shows the amount of
alcohol contained in the vapors given off from alcoholic liquids of
different strength, and also their boiling points.
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