Detection of the Common Food AdulterantsBruce, Edwin M.
Science
Detection of the Common Food Adulterants
Bruce, Edwin M.
Food adulteration and inspection
_Hess and Doolittle Test._--Melt some of the butter (say 40 grams) at
about 50° C. If the butter is pure and fresh the melted fat will clear
up almost as soon as it is melted, while the fat of process butter
remains turbid for quite a while. After most of the curd has settled,
decant as much as possible of the fat. Pour the remainder on a wet
filter. Add a few drops of acetic acid to the water that runs through
from the filter, and boil. If it was ordinary butter this filtrate will
become milky, but if process butter a flocculent precipitate will form.
OLEOMARGARINE
Immerse a test tube, containing some of the filtered fat, in boiling
water for 2 minutes. Make a mixture of 1 part glacial acetic acid, 6
parts ether, and 4 parts alcohol. Add to 20 cc. of this mixture in a 50
cc. test tube, 1 cc. of the heated fat which may be transferred by means
of a hot pipette. Stopper the tube and shake it well. Immerse in water
at 15° or 16° C. Pure butter when thus treated remains clear for quite a
while. There will be only a very little deposit after standing an hour,
but oleomargarine gives a deposit almost immediately, and in a few
minutes there will be a copious precipitate.
When the oleomargarine in butter is in about the proportion of 1 : 10,
it will not separate much short of 15 minutes.
COTTONSEED OIL
The presence of this oil may be detected by Halpen’s test, which is
given under lard, page 60.
CHAPTER II
MEATS AND EGGS
Meats are preserved by treating them with potassium nitrate, boric acid,
sulfurous acid, salicylic acid, or benzoic acid. Cheap meat may be
substituted for the more expensive. A few cases of horse meat in mince
meat and sausages have been discovered. Diseased and stale meats have
been found on the market. Canned meats often contain zinc, tin, and
lead, and sometimes even arsenic. Aniline-red or cochineal-carmine may
be added to improve the color of chopped or ground meats. Starch is
sometimes added to sausage and similar meat. Fish and oysters may be
preserved with boric acid or borax.
FRESH AND SMOKED PRODUCTS--PRESERVATIVES
POTASSIUM NITRATE (SALTPETER)
Corned and smoked meats are usually preserved with saltpeter. Since
smoked and cured meats are used in making potted meats, saltpeter is
quite frequently found in the latter. It may be detected by the usual
test for nitrates since no other nitrate is apt to be present, though
one may identify the metal by the qualitative test for potassium.
To test for nitrates treat a little of the meat with 2 or 3 cc. of a 1
per cent solution of diphenylamine in strong sulfuric acid. If a
nitrate is present a deep blue color forms instantly, which is not
obscured by the charring effect of the acid.
BORIC ACID
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account