Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant. — John Shaqi
Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant.Thomssen, Edgar George
Science
Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant.
Thomssen, Edgar George
Soap
Na_{2}Cr_{2}O_{7} + 8HCl = Cr_{2}Cl_{6} + 2NaCl + 7O.
in which the oxygen is the active principle. In practice it is found
necessary to use an excess of acid over that theoretically indicated.
For the best results an oil should be chosen containing under 2 per
cent. impurities and a low percentage of free fatty acids. Lagos oil is
best adapted to these requirements. The oil is melted by open steam from
a jet introduced through the bung, the melted oil and condensed water
running to the store tank through two sieves (about 1/8 inch mesh) to
remove the fibrous material and gross impurities. The oil thus obtained
contains fine earthy and fibrous material and vegetable albuminous
matter which should be removed, as far as possible, since chemicals are
wasted in their oxidation and they retard the bleaching. This is best
done by boiling the oil for one hour with wet steam and 10 per cent.
solution of common salt (2 per cent. dry salt on weight of oil used) in
a lead-lined or wooden tank. After settling over night the brine and
impurities are removed by running from a cock at the bottom of the vat
and the oil is run out into the bleaching tank through an oil cock,
situated about seven inches from the bottom.
The bleaching tank is a lead-lined iron tank of the approximate
dimensions of 4 feet deep, 4 feet long and 3-1/2 feet wide, holding
about 1-1/2 tons. The charge is one ton. A leaden outlet pipe is fixed
at the bottom, to which is attached a rubber tube closed by a screw
clip. A plug also is fitted into the lead outlet pipe from above. Seven
inches above the lower outlet is affixed another tap through which the
oil is drawn off.
The tank is further equipped with a wet steam coil and a coil arranged
to allow thorough air agitation, both coils being of lead. A good
arrangement is to use one coil to deliver either air or steam. These
coils should extend as nearly as possible over the entire bottom of the
tank and have a number of small downward perforations, so as to spread
the agitation throughout the mass.
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