Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant.Thomssen, Edgar George
Science
Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant.
Thomssen, Edgar George
Soap
To make a semi-boiled soap, using any of the above formulae, first melt
the rosin with all or part of the fat, as rosin when melted alone
readily decomposes. When the mixture is at 150deg. F. run it into the
crutcher and add the lye. Turn on sufficient dry steam to keep the
temperature of the soap at about 150deg. F. in the winter or 130deg. F. in
summer. After the mass has been mixed for half an hour, by continuously
crutching the soap it will at first thicken, then grain and it may again
become thick before it becomes smooth. When the mass is perfectly smooth
and homogeneous drop into a frame and crutch in the frame by hand to
prevent streaking. After standing the required length of time the soap
is finished into cakes as usual.
SETTLED ROSIN SOAP.
Settled rosin soaps are made from tallow, grease, cottonseed oil,
bleached palm oils of the lower grades, corn oil, soya bean oil, arachis
oil, distilled garbage grease, cottonseed foots or fatty acids together
with an addition of rosin, varying from 24 per cent. to 60 per cent. of
the fatty acids which should titer from 28 to 35. A titer lower than 28
will prevent the finished kettle of soap from being capable of later
taking up the filling materials. As has already been stated under
hardened oils, these being very much higher in titer allow a greater
percentage of rosin to be added. Thus hardened fish oils and cottonseed
oil are gradually being more extensively employed in soaps of this
character.
The procedure of handling the kettle is similar to that given under full
boiled soap. The stock is steamed out into a settling tank and allowed
to settle over night, after which it is pumped into the soap kettle.
Having stocked the kettle, open steam is turned on and 10deg.-12deg. B.
lye is run in, while using a steam pressure of ninety to one hundred
pounds in order to prevent too great a quantity of condensation of the
steam, the water thus being formed weakening the lye. If a steam
pressure of fifty to sixty pounds is available, a stronger lye (20deg.
B.) should be added. Care must be taken not to allow the lye to flow in
too rapidly or the soap will not grain. The saponification is only
attained by prolonged boiling with sufficient lye of proper strength.
When saponification has taken place, the mass begins to clear and a
sample taken out with a paddle and cooled should show a slight pink with
a 1 per cent. alcoholic phenolphthalein solution.
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