Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant.Thomssen, Edgar George
Science
Soap-Making Manual: A Practical Handbook on the Raw Materials, Their Manipulation, Analysis and Control in the Modern Soap Plant.
Thomssen, Edgar George
Soap
It may be stated here that in using this indicator or any other to test
the alkalinity of soap, the soap should always be cooled and firm, as
whenever water is present, the dissociation of the soap thereby will
always react alkaline. When this state is reached the mass is ready for
graining, which is accomplished by distributing salt brine or pickle or
spreading dry salt over the surface of the soap. The kettle is then
thoroughly boiled until the mass shows a soft curd and the lye drops
clearly from a sample taken out with a trowel or paddle. The steam is
then shut off and the soap allowed to settle over night. The lyes are
then run off to the spent lye tank for glycerine recovery. In
saponifying a freshly stocked kettle it is apt to bunch. To prevent this
salt is added at various times to approximately one per cent. of the fat
used.
If, by any possibility the soap has bunched, this condition may be
remedied by the addition of more strong lye and boiling until it is
taken up. To work a kettle to its full capacity it is advisable to make
two "killing" changes. First add about 75 per cent. of the fat and grain
as directed. Run off the spent lyes and then add the remainder of the
stock and repeat the process. When the spent lye has been run to
storage, the open steam is again turned on and 18deg. B. lye gradually
allowed to run in. The rosin is now broken up and put into the kettle,
or a previously made rosin soap is pumped in.
Lye is then added until the soap has a sharp taste after about three
hours of continuous boiling, or when the soap is in the closed state.
More lye should then be run into the kettle to grain the soap well, the
grain not being too small. Then allow the soap to settle over night and
draw off the strengthening lye. The next day again boil up the kettle
and add water until the soap thins out and rises or swells high in the
kettle. A sample taken out at this stage upon a hot trowel should run
off in large flakes. The surface of the soap should be bright and shiny.
If the sample clings to the trowel, a slight addition of lye will remedy
this defect. The kettle is then allowed to rest, to drop the nigre and
to cool for some time, depending upon the size of the kettle. The proper
temperature is such that after having been pumped to the crutcher and
the filling materials having been added, a thermometer placed into the
mass should indicate 128deg.-135deg. F. after the crutcher has run from
ten to fifteen minutes. The filling material may consist of from 7-9 per
cent. of sal soda solution, 36deg.-37deg. B. warm or just enough to
close up the soap and make it rise high in the center of a screw
crutcher and make it cling close to a warm trowel. Other fillers such as
outlined below are added at this point.
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